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i <br /> 110 2nd Avenue Soutb,#D7,Pacheco,CA 94553-5560 <br /> E A <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mcc bell corn E-mail ma bell coin <br /> • 7- <br /> Robert A Booher Consulting Client Protect ID #CC-103, Cal Cedar Date Sampled 07/21/03 <br /> 3247 Glen Abby Drive 1340 W Washington Stockton CA Date Received 07/23/03 <br /> Fairfield, CA 94533 Client Contact Jeff Monroe Date Extracted 07/23/03 <br /> I <br /> Client P O Date Analyzed 07124/03-07/26/03 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel* <br /> xtiactwnnxtlin& SW3550C Analytical methods SW8015C Work Order 0307385 <br /> Lab ID Client ID Matrix TPH(d) DF %SS <br /> 0307385-0112A HP-2-22 5' S ND 1 973 <br /> 0307385-003B HP-2-W W ND,i 1 996 <br /> I 0307385-005A HP-4-24 0' S ND 1 962 <br /> 0307385-006B HP-4-W W 87,b,i 1 102 <br /> 0307385-008A HP-5-24 0' S ND 1 940 <br /> 0307385-009B HP-5-W W 1700,g,i 20 101 <br /> I 0307385-012A HP-3-23 0' S 51,d 1 120 <br /> 0307385-013B I P-3-W W 430,9,b,i 1 105 <br /> 0307385-OISA HP-1-24 0' S 2 4,d 1 950 <br /> 0307385.016B HP-1-W W 4300,d,i 1 105 <br /> I0307385-017A HP-1-33 0' S ND 1 971 <br /> Reporting Limit for DF=1, W 50 gg/L. <br /> ND means not detected at or <br /> above the reporting limit S 1 0 mg/Kg <br /> "water samples are reported in pg/L,wipe samples in gg/wipe,saillsolid/sludge samples to mg/kg,productloiUnon-aqueous liquid samples in mg/L,and <br /> all DISTLC/STLC/SPLP 1 TCLP extracts are reported inµg/L <br /> #cluttered chromatogram resulting in coeluted surrogate and sample peaks,or,surrogate peak is on elevated baseline,or,surrogate has been diminished <br /> by dilution of original extract <br /> I +The following descriptions of the TPFI chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation a) <br /> unmodified or weakly modified diesel is significant,b)diesel range compounds are significant,no recognizable pattern,c)aged diesel?is significant),d) <br /> gasoline range compounds are significant,e)unknown medium boiling point pattern that does not appear to be derived from diesel,f)one to a few <br /> isolated peaks present,g)oil range compounds are significant,h)lighter than water immiscible sheen/product is present,i)liquid sample that contains <br /> Igreateir than—2 vol %sediment,k kerosene/kerosene range,I bunker oil,m fueI oil,n Stoddard solvent/mineral spirit <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br /> I <br />