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A8L1471 Ekiiiiiiiiiiiiilli General: Heavy Metals ASSOCIATES BSK Associates Laboratory Fresno Metals Quality Control Report Spike Source %REC RPD Date Analyte Result RL Units Level Result %REC Limits RPID Limit Analyzed Qual EPA 6020-Quality Control Batch:A818733 Prepared: 12/15/2018 Prep Method:EPA 3010A for STLC/DISTLC Analyst: MAS Blank Spike(A818733-BS1) Lead,WET 7.7 0.25 mg/L 8.0 ND 96 75-125 12/17/18 Molybdenum,WET 9.0 0.50 mg/L 8.0 ND 113 75-125 12/17/18 Nickel,WET 7.9 0.50 mg/L 8.0 ND 99 75-125 12/17/18 Selenium,WET 8.0 0.10 mg/L 8.0 ND 100 75-125 12/17/18 Silver,WET 3.7 0.50 mg/L 4.0 ND 93 75-125 12/17/18 Thallium,WET 7.8 0.50 mg/L 8.0 ND 97 75-125 12/17/18 Vanadium,WET 8.7 0.50 mg/L 8.0 ND 109 75-125 12/17/18 Zinc,WET 7.5 2.5 mg/L 8.0 ND 93 75-125 12/17/18 Blank Spike Dup(A818733-BSD1) Antimony,WET 8.4 0.50 mg/L 8.0 ND 106 75-125 1 20 12/17/18 Arsenic,WET 8.6 0.10 mg/L 8.0 ND 107 75-125 3 20 12/17/18 Barium,WET 7.9 0.25 mg/L 8.0 ND 98 75-125 0 20 12/17/18 Beryllium,WET 7.8 0.050 mg/L 8.0 ND 98 75-125 1 20 12/17/18 Cadmium,WET 7.7 0.050 mg/L 8.0 ND 97 75-125 1 20 12/17/18 Chromium,WET 8.4 0.50 mg/L 8.0 ND 105 75-125 1 20 12/17/18 Cobalt,WET 8.2 2.5 mg/L 8.0 ND 102 75-125 1 20 12/17/18 Copper,WET 7.9 0.50 mg/L 8.0 ND 98 75-125 1 20 12/17/18 Lead,WET 7.6 0.25 mg/L 8.0 ND 95 75-125 1 20 12/17/18 Molybdenum,WET 8.9 0.50 mg/L 8.0 ND 111 75-125 1 20 12/17/18 Nickel,WET 8.2 0.50 mg/L 8.0 ND 102 75-125 3 20 12/17/18 Selenium,WET 7.8 0.10 mg/L 8.0 ND 98 75-125 2 20 12/17/18 Silver,WET 3.7 0.50 mg/L 4.0 ND 93 75-125 1 20 12/17/18 Thallium,WET 7.7 0.50 mg/L 8.0 ND 96 75-125 1 20 12/17/18 Vanadium,WET 8.7 0.50 mg/L 8.0 ND 109 75-125 0 20 12/17/18 Zinc,WET 7.5 2.5 mg/L 8.0 ND 93 75-125 0 20 12/17/18 Duplicate(A818733-DUP1),Source:A8L1471-01 Antimony,WET ND 0.50 mg/L ND 20 12/17/18 Arsenic,WET 0.51 0.10 mg/L 0.52 2 20 12/17/18 Barium,WET 7.0 0.25 mg/L 7.7 9 20 12/17/18 Beryllium,WET ND 0.050 mg/L ND 20 12/17/18 Cadmium,WET ND 0.050 mg/L ND 20 12/17/18 Chromium,WET ND 0.50 mg/L ND 20 12/17/18 Cobalt,WET ND 2.5 mg/L ND 20 12/17/18 Copper,WET ND 0.50 mg/L ND 20 12/17/18 Lead,WET ND 0.25 mg/L ND 20 12/17/18 Molybdenum,WET ND 0.50 mg/L ND 20 12/17/18 Nickel,WET ND 0.50 mg/L ND 20 12/17/18 Selenium,WET ND 0.10 mg/L ND 20 12/17/18 Silver,WET ND 0.50 mg/L ND 20 12/17/18 Thallium,WET ND 0.50 mg/L ND 20 12/17/18 Vanadium,WET 16 0.50 mg/L 18 12 20 12/17/18 Zinc,WET ND 2.5 mg/L ND 20 12/17/18 Matrix Spike(A818733-MS1),Source:A81-1471-01 The results in this report apply to the samples analyzed in A811471 FINAL 12272018 1717 accordance with the chain of custody document. This analytical report must be reproduced in its entirety. www.BSKAssociates.com Page 10 of 18