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- - 0,' MAUM VERIFICATION LABORATORY ANALYSIS <br /> PCB <br />' TANK TANK TP"-G TPH-D BTX & E CL HC TOTAL EDB CAP; 8270 <br /> 8015 8015 8020 8010 LEAD 8080 <br /> # CONTENTS 826(1 8240 7420 8240 AFS or <br /> 8260 8260 7421 AA <br /> O ' LEADED X X X <br /> 1 GAS X <br /> X <br /> 5 <br /> DIESEL X X <br /> KEROSENE X X <br />' X <br /> UNK FUEL X <br /> X X X <br /> PROD OIL X X <br /> C14LOR X X <br /> SOLVENTS <br /> NONCHLOR X X X <br />' SOLVENT'S <br /> W ASM X X X <br /> USED OIL X X X <br />' methods described in EPA SW 846, Third Edition. Those methods not found <br /> All analyses methods are designated EPA m Appendix A-20, Table 3-5 for <br /> in SW 846, are specifically noted below Refer to the 'SWRCB Refer <br /> t 1' Field Manual", <br /> detection limits of motor vehicle fuels (gasoline and diesel) Ref oto[ oil deteclgon limional its Staff Recommendations far <br /> Initial Evaluation and Investigation of UST's for the waste and m question will be accepted, <br /> T)etection Limits that remain below the M o sorra;e N}°�Allowable limit o[ the contaminant in <br /> however lnboratory shall utilize <br /> LABORATORY ANALYSIS TERMINOLOGY 5030 8015 mod or GCIMS 8260 <br /> TPN G Total Petroleum Hydrocarbon, Ga.Soline, GClF1D015 mod or GCIMS 8260 <br /> ' 7 p}l_D Total Petroleum Hydrocarbon, Diesel, GCJFID (3550), 8 <br /> SIX & E Benzene, Toluene, Xylene & Ethyl Benzene, GGP 8 48020 or GC/MS 8260 <br /> ' <br /> CL HC Chlorinated Hydrocarbon, G(:IHSD 8o10, GC M Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> `I O HC LEAD <br /> EDB Ethylene dibromide (DHS-AB 1803), GC/M <br /> S20 DHS-LUPI) <br /> ED FID Gas Chromatography, Flame ionization Detection <br /> /CAP or AA Inductively Coupled Plasma Ato Calm[Emission <br /> ChromlSpectum III/rometry 6d0 V110, <br /> PCB <br /> Zine andr Atomic Nickel. <br /> Spectrometry 7000 Metals <br /> PCB Polychlorinated Biphenyls, GAMS 8270 or 8080 <br /> ' <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparation <br /> ' QA/QC Quality Assurance/Quality t;.ontro! <br /> ts are be <br /> Fused <br /> pillary <br /> are <br /> Notes To avoid false positive detection of benzene, benzene-frfirst cut" withodtrtysOlvcn " samples or ante the hydoca bons <br /> ' preferred to packed columns, a packed column may be used as o <br /> have been characterized and proper QAIAC is followed In preference to the 600 <br /> tile organics for <br /> For Drinking water sources, EPA recommends that the 500 setibbett ryola Samples exhibiting any level of heavy metal <br /> ( series because the detection limits are lower and the QAIQC Is <br /> contamination may require further analysts PHS-EHD recommends holding these samples until disposal Is Indicated. <br /> EH 23 048 (Revised 7/10/92) Page 8 <br /> 51.1 C0-4&r (i� Grin <br />