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QUALITY ASSURANCE REPORT <br /> Z� SPIKE DUPLICATE RESULTS <br /> Client Lab Number QSD VS21226 <br /> ZymaX envirotechnology, inc Collected <br /> 71 Zaca Lane, Suite 110 Received <br /> San Leis Obispo, CA 93401 Matrix Soil <br /> Project Sample Description <br /> Quality Assurance Spike Duplicate <br /> Project Number Analyzed 12/26/02 <br /> Collected by Method See Below <br /> CONSTITUENT Amount Spiked Amount Recovered Percent Relative Percent <br /> mg/kg mg/kg Recovery Difference* <br /> Benzene 0 038 0 040 105 3 <br /> Toluene 0 060 0 068 113 3 <br /> Ethylbenzene 0 040 0 042 105 2 <br /> Xylenes 0 093 0 099 106 4 <br /> Methyl t-Butyl Ether (MTBE) 0 127 0 143 113 7 <br /> Percent Surrogate Recovery 108 <br /> TOTAL PETROLEUM HYDROCARLJONS <br /> Gasoline 1 67 1 60 96 4 <br /> OBTX as a Percent of Fuel 11 13 <br /> ZymaX envirotechnology, inc is certified by CA Department of Health Services Laboratory #1717 <br /> *Relative Percent Difference of the spike and spike duplicate <br /> Note Analyzed by EPA 8260 and GC/MS Combination <br /> Submitted by, <br /> ZymaX envirotechnology, inc <br /> VS21226 <br /> MSD #2 '7 <br /> VS21226q xls Dwain Zsadanyl <br /> DZ/ashlpv Project Manager <br /> `° Lone <br /> 805 544 4696 <br /> pan Luis Ol7isDo CA 93407 <br /> varVvv71fM aX,[.iSa 0C)M a 805 544 8226 <br />