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110 2nd Avenue South 4D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> http 1/www mceampbell cam Email mamEmccampbel I com <br />' Advanced GeoEnvironmental, Inc Client ProjeLt ID Marlowe Prop Date Sampled 06/18/03 <br /> • 837 Shaw Road Date Received 06/24/03 <br />' Stockton, CA 95215 Client Contact Brian Millman Date Extracted 06128103-07/01/03 <br /> Client P O Date Analyzed 06/28/03.07/01/03 <br />' Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0306497 <br />' Lab ID 0306497-OOIC 0306497-0020 0306497-003C 0306497-004C <br /> Chent ID MW1/06-18-03 MW5/06-18-03 MW6/06-18-03 VW-1/06-18-03 <br /> Reporting Limit for <br /> IMatrix -----W ---- ----W-__ - I ----W---------- W DF=1 <br /> DF 1 1 I 1 1 S W <br /> I I <br /> Compound Concentration ug/kg µg/L <br /> Dusopropyl ether(DIPE) ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> • t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 05 <br /> 1 2-Dichloroethane(1,2-DCA) 13 17 12 i 54 NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 120 115 115 102 <br /> Comments <br /> I <br /> *water and vapor samples and all TCLP&SPLP extracts are reported toµg/L soil/sludge/solid samples inµg/kg, wipe samples in pg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> END means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydebus, Lab Manager <br /> f <br />