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Excelchem Environmental Labs <br /> Ramage Environmental Project SJ County Courthouse <br /> 465 South Meadows Parkway Suite 20 pmb 48 Project Number NA Date Reported <br /> Reno NV, 8952! Project Manager Joe Ramage 03/23/06 13 26 <br /> Oxygenates- Quality Control <br /> Analyte Rep rlin S�pikg Source /o C �p <br /> Result limit Units Leve Result % C Limts RPD Limit Notes <br /> Batch APC0091 -EPA 8260B <br /> Blank(APC0091-BLK1) Prepared 03/20/06 Analyzed 03/21/06 <br /> Surrogate Dihromofluoromethane 128 ug/l 125 102 70-130 <br /> Surrogate Toluene-d8 124 125 992 70-130 <br /> Surrogate 4-Bromofluorobenzene 139 125 111 70-130 <br /> Ethanol ND 200 " <br /> TBA ND 50 " <br /> Methyl tert-Butyl Ether ND 05 " <br /> Di-isopropyl ether ND 05 " <br /> Ethyl teri-Butyl Ether ND 05 " <br /> Tert-Amyl Methyl Ether ND 05 <br />' 1,2-Dichloroethane ND 05 <br /> 1,2-Dibromoethane(EDB) ND 05 " <br /> LCS(APC0091-BSI) Prepared 03/20/06 Analyzed 03/21/06 <br /> gale Dibromofluoromethane 125 u9/1 125 100 70-130 <br /> rogate Toluene-d8 120 125 960 70-130 <br /> Surrogate 4-Bromofluorobenzene 147 125 118 70-130 <br /> 1,1-Dichloroethene 9'4 05 11 100 940 20-120 <br /> Benzene 9 3 05 100 93 0 20-120 <br /> Trichloroethene 9 1 0 5 10 0 91 0 20-120 <br />'Toluene 9 4 0 5 10 0 94 0 20-120 <br /> Chlorobenzene 8 7 0 5 too 870 20-120 <br /> Matrix Spike(APC0091-MSI) Source 0603064-03 Prepared 03/20/06 Analyzed 03/21/06 <br /> Surrogate Dibromofluoromethane 129 ug/I 125 103 70-130 <br /> Surrogate Toluene-48 122 125 976 70-130 <br /> Surrogate 4-Bromofluorobenzene 138 123 110 70-130- <br /> 1 1-Dichloroethene 10'2 0 5 loo ND 102 20-120 <br /> Benzene 9 6 0 5 100 ND 960 20-120 <br /> Trichloroethene 9 0 05 100 ND 900 20-I20 <br /> Toluene 94 0 5 too ND 94 0 20-120 <br /> floroberizene 93 05 100 ND 93 0 20-120 <br /> r <br /> lchem Environmental Lab The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br />' Laboratory Representative Page 5 of 9 <br />