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A i•ican Env'i o/i/nental Neri1 of WORK ORDER: 9710182 � � QUALITY CONTROL REPORT PAGE QR-5 ANALYSIS: Metal's Scan by ICP MATRIX: Pater METHOD BLANK "SAMPLES , i INSTRUMENT: BlaTJA E ------ ........................... TYPE: Blank' Method/Media blank PREPARED: •--------------------------•-------•--•---- nviro 36 LAB ID: IFW PBW Q INSTR RUN: ICP\971017135100/1/ i UNITS: mg/L ' ANALYZED: 10/17/97 BATCH ID: IFW101697•Q METHOD: DILUTION: 1.000000 i ANALYTEREF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD Ag Silver ' RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (1) LIMIT (X) NO 0.005 Al Aluminum ND 0.1 Ba Barium ND 0.01 Be Beryllium NO 0.002 ! Cd Cadmium NO 0.005 Co Cobalt ND 0.005 Cr Chromium ND 0.01 Cu Copper- NO 0.01 Mo Molybdenum NO 0.01 Ni Nickel ND 0.01 Pb Lead NO 0.04 Sb Antimony NO 0.02 Tl Thallium ND 0.05 V Vanadium NO 0.005 Zn Zinc NO 0.01 •----------------•-----••-•----•---------.........-,--•--------•--------•------•-•--••......••--•-......- LABORATORY CONTROL SAMPLES ------•-•---....--•••-•._...•_•. ---•-••...-------•••••----••--- INSTRUMENT: TJA Enviro 36 PREPARED: =Q INSTRATCH RUN: ICP\971017135100/3/1 BATCH ID: IFW10160171 SAMPLE TYPE: Spike-Method/Media blank LAB ID: IFW LCD UNITS: mg/L ANALYZED: 10/17/97 DILUTION: 1.000000 METHOD: REF REPORTING SPIKE',] RECOVERY REC LIMITS (X) RPD t ANALYTE RESULT RESULT LIMIT VALUES (X) LOW HIGH RPD (X) LIMIT (X) Ag Silver 0.0240 NO 0.005 0.0250 '' 96.0 72 127 Al Aluminum 1.06 ND 0.1 1.00 106 89 116 Ba Barium 1.03 NO 0.01 1.00 L; 103 91 120 Be Beryllium 0.0268 NO 0.002 0.0250 107 82 119 Cd Cadmium 0.0508 NO 0.005 0.0500 !1 102 84 120 E Co Cobalt 0.269 NO 0.005 0.250108 96 120 I Cr Chromium 0.104 NO 0.01 0.100 !lit 104 85 128 Cu Copper 0.117 NO 0.01 0.125 I,; 93.6 86 123 Mo Molybdenum 0.207 NO 0.01 0.200 104 89 117 Ni Nickel 0.272 NO 0.01 0.250 109 92 121 L Pb Lead 0.538 ND 0.04 0.500 L'v 108 90 122 Sb Antimony 0.510 NO 0.02 0.500 'N 102 82 113 T1 Thallium 0.496 NO 0.05 0.500 Ii 99.2 85 115 V Vanadium 0.261 NO 0.005 0.250 104 91 118 Zn Zinc 0.252 NO 0.01 0.250 101 90 121 ................. _..._....._..... .. __.............___.__............__._.. .................. .--....•.....---......--._.._...................... _.....__._...._____.....___..._.................._. SAMPLE TYPE: Spike-Method/Media blank LAB ID: IFW LCS_Q INSTR RUN: ICP\971017135100/2/1 INSTRUMENT: TJA Enviro 36 PREPARED: BATCH ID: IFW101697-Q UNITS: mg/L ANALYZED: 10/17/97 DILUTION: 1.000000 METHOD: 11 { REF REPORTING SPIKE.: RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE'; (X) LOW HIGH RPD (X) LIMIT (X) Ag Silver 0.0255 NO 0.005 0.0250 11 102 72 127 Al Aluminum 1.02 NO 0.1 1.00 102 89 116 Ba Barium 1.00 ND 0.01 1.00 'ii 100 91 120 Be Beryllium 0.0259 NO 0.002 0.0250 'i 104 82 119 Cd Cadmium 0.0492 NO 0.005 0.0500 98.4 84 120 i (( Co Cobalt 0.264 NO 0.005 0.250 'I 106 96 120 L Cr Chromium 0.0996 NO 0.01 0.100 99.6 85 128 Cu Copper 0.116 NO 0.01 0.125 ii 92.8 86 123 1 Mo Molybdenum 0.201 NO 0.01 0.200 '; 101 89 117 Ni Nickel 0.265 ND 0.01 0.250 106 92 121 Pb Lead 0.526 NO 0.04 0.500 105 90 122 Sb Antimony 0.502 NO 0.02 0.500 ; 100 82 113 Tl Thallium 0.474 NO 0.05 0.500 94.8 85 115 V Vanadium 0.257 NO 0.005 0.250 103 91 118 I�