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11 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone :925-798-1620 Fax-,925-798-1622 <br /> htt :// vww.mccam bell.com E-mail:main2mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Manteca City Yard Date Sampled: 08/05/99 <br /> 4005 North Wilson Way Date Received: 08/06,199 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 08/06/99 <br /> Client P.O: Date Analyzed: 08/06/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 16754 16755 16756 16757 <br /> Reporting Limit <br /> Client 1D TK 2A TK 2B TK 3A TK 3B <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPL) ND<15 ND ND ND 5.0 Lo <br /> Ethyl tert-Butyl Ether(ETRE) IT'D<€5 ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) 320 ND ND 7.1 5.0 1.0 <br /> tert-Amy] Methyl Ether(TAME) ND<15 ND ND ND 5.0 lA <br /> E, <br /> tert-Butanol ND<73 ND ND ND 25 5.0 <br /> i <br /> Surro�ate Recoyeri s(%) <br /> I <br /> Dibromotluoromethane 99 90 97 96 <br /> I <br /> I <br /> Comments: <br /> I <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg.H ipes n ug/wipe and all TCLP!STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit:N/A means surrogate not ap licable to this analysis <br /> (h)lighter than water immiscible sheen is present:(i)liquid sample that cont ins greater than—5 vol."o sediment:0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />