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1 <br /> 110 2nd Avenue South #D7,Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-79s-1622 <br />' <br /> http//wwwrnccanipbel1com E-mail mainArnecanipbellcorn. <br /> Advanced GeoEnvironmental,Inc Client Project ID Manteca Corp Yard Date Sampled 02/19/03 <br />' 837 Shaw Road Date Received 02/20/03 <br /> Stockton,CA 95215 Client Contact Brian Millmmn Date Extracted 02/20/03 <br />' <br /> Lch--rntp <br /> O Date Analyzed 02/21/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analybcal Method SW8260B Work Order 0302269 <br /> Lab ID 0302269-002A 0302269-004A 0302269-006A 0302269-007A <br /> Client ID MW8-15 MW8-25 MW9-15 MW9-25 Reporting Limit for <br />' Matrix S �-- -- S �-� S S DF=1 <br /> DF 1 I I 1 S W <br /> i <br /> Compound Concentration gg/Kg ug/I. <br /> tett-Amyl methyl ether(TAME) ND ND ND ND 50 NA <br /> Benzene ND ND ND ND 5 0 NA <br /> t-Butyl alcohol(TBA) ND ND ND ND 25 NA <br /> 1 2-Dtbromoethane(EDB) ND ND ND ND 5 0 NA <br /> 1,2-Dtchloroethane(1,2-DCA) ND ND ND ND 5 0 NA <br /> Dnsopropyl ether(DIPS) ND ND — ND ND 50. NA <br /> Ethylbenzene ND ND ND ND 5 0 NA <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND 5 0 NA <br /> Methyl-t-butyl ether(MTBE) ND ND ND 64 50 NA <br /> Toluene ND ND ND ND 5 0 NA <br /> Xylenes ND ND ND ND 5 0 NA <br /> Surrogate Recoveries{%) <br /> %SSI 104 104 106 104 <br /> Comments -7 <br /> •water and vapor samples and all TCLP&SPLP extracts are reported to Ag/L,sotUsludge/soltd samples in gglkg, wipe samples to Ag/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than-2 vol %sediment,I)sample diluted due to high <br /> organic content <br /> I <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />