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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCAUTBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Ihttp//www mccampbell com E-mail matn@mccampbell com <br /> IAdvanced GeoEnvironmental Client Project 1D Manteca Corp Yard Date Sampled 0110$-01/09102 <br /> 837 Shaw Road Date Received 01/10/02 <br />' Stockton, CA 95215 Client Contact Brian Millman Date Extracted 01/10/02 <br /> Client P O Date Analyzed 01/10/02 <br />' Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* & BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602,California RWQCB(SF Bay Region)method GCFID(5030) <br /> Ethyl- %Recovery <br />' Lab 1D Client ID Matrix TPH(g) MTBE Benzene Toluene Xylenes <br /> benzene Surrogate <br /> 88049 CPTI H20- W ND --- ND ND ND ND 93 <br /> 41-45 <br />' 88050 CPTI HZO- W ND --- ND ND ND ND 100 <br /> 64-68 <br /> 88051 CPTI H2O- W ND --- ND ND ND ND 99 <br /> 82-86 <br />' 88052 CPTI-35 S ND --- ND ND ND ND 101 <br /> 88053 CPT2 HO- W ND --- ND ND ND ND 100 <br /> 41-45 <br /> 88054 CPT2 HZ --- <br /> O- W ND ND ND ND ND 97 <br /> 64-68 <br /> 88055 CPT2 H20- W ND --- ND ND ND ND 105 <br /> 79-83 <br /> 88056 CPT3 H2O- W ND _-- <br /> ND ND ND ND 104 <br /> 41-45 <br />' 88057 CPT3 H2O- W ND -- ND ND ND ND 105 <br /> 64-68 <br /> 88058 CPT3-HO- W ND _— ND ND ND ND 102 <br /> 81-85 <br /> Reporting Limit unless W 50 ug/L 5 0 05 05 05 05 <br /> otherwise stated,ND <br /> means not detected above S 1 0 mg/kg 0 05 0 005 0 005 0 005 0 005 <br />' the reporting limit <br /> 'water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br />' a cluttered chromatogram sample peak coelutes with surrogate peak <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are significant(aged <br />' gasoline-?), 0 lighter gasoline range compounds (the most mobile fraction) are significant d) gasoline range compounds having broad <br /> chromatographic peaks are significant biologically altered gasoline9,e)TPH pattern that does not appear to be derived from gasoline(?),f) <br /> one to a few isoiated peaks present,g) strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible <br /> sheen is present,i)liquid sample that contains greater than—5 vol %sediment,j)no recognizable pattern <br />' DHS Cerhf-ication No 1644 Edward Hamilton,Lab Director <br />