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Alpha Analytical, Inc.
<br /> 255 Glendale Ave.•Suite 21 a Sparks,Nevada 89431-5778
<br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183
<br /> Date: Work Order:
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<br /> 03- „r-la QC Summary Report 14032043
<br /> Method Blank Type MBLK Test Code: EPA Method 200.8
<br /> Pile ID: 061 Batch ID:32636 Analysis Date: 03126/2014 21:00
<br /> Sample ID. MB-32636 Units:pg/L Run ID:ICPIMS 140325C Prep Dale: 03/2412014 15:43
<br /> Analyte Result PQL SpkVal SpkRefVal%REC LCL(ME) UCL(ME)RPDRefVal %RPD(Liri Qual
<br /> Magnesium(Mg),Dissolved NO 500
<br /> Calcium(Ca),Dissolved NO 500
<br /> Chromium(Cr),Dissolved ND 10
<br /> Manganese(Mn),Dissolved ND 5
<br /> Nickel(Ni),Dissolved ND 10
<br /> Copper Cu),Dissolved NO 20
<br /> Arsenic(As),Dissolved NO 5
<br /> Molybdenum(Mo),Dissolved NO 5
<br /> Cadmium(Cd), Dissolved ND 2
<br /> Barium(Be),Dissolved NO 5
<br /> Mercury(Hg),Dissolved NO 1
<br /> Lead(Pb) Dissolved NO 5
<br /> Laboratory Control Spike Type LCS Test Code: EPA Method 200.8
<br /> File ID'. 083_ Batch ID:32636 Analysis Date: 0312512014 21:08
<br /> i Sample ID. LCS-32636 Units: pg1L Run ID:ICPIMS_140325C Prep Date: 03/2412014 15:43
<br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRe'Val %RPD(Urnit) Qual
<br /> Magnesium(Mg),Dissolved 4740 500 5000 95 80 120
<br /> Calcium(Ca),Dissolved 4430 500 5000 89 80 120
<br /> Chromium(Cr),Dissolved 47.8 10 50 96 80 120
<br /> Manganese(Mn),Dissolved 488 5 500 98 80 120
<br /> Nickel(Ni),Dissolved 47.4 10 50 95 80 120
<br /> Copper(Cu),Dissolved 48.1 20 50 96 8o 120
<br /> Arsenic(As),Dissolved 49.9 5 50 99.8 80 120
<br /> Molybdenum(Mo),Dissolved 45.5 5 50 91 80 120
<br /> Cadmium(Cd),Dissolved 47.2 2 50 94 80 - 120
<br /> Barium(Be),Dissolved 47.5 5 50 95 80 120
<br /> Mercury(Hg),Dissolved 0.9 1 1 90 80 120
<br /> Lead(Pb),Dissolved 47.1 5 50 94 80 120
<br /> Sample Matrix Spike Type MS Test Code: EPA Method 200.8
<br /> File ID: 065_ Batch ID'.32636 Analysis Date: DY2612014 21:12
<br /> Sample ID: 14031324-OIAMS Units:pi Run ID:ICP/MS.140325C Prep Date: 0312412014 15:43
<br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDReNaI %RPD(Limtt) Qual
<br /> Magnesium(Mg),Dissolved 63700 500 5000 59840 76 75 125 M3
<br /> Calcium(Ca),Dissolved 122000 500 5000 118300 65 75 125
<br /> Chromium(Cr),Dissolved 62.7 10 50 15.5 94 75 125
<br /> Manganese(Mn),Dissolved 462 5 500 0 92 75 125
<br /> Nickel(Ni),Dissolved 46.1 10 50 0 92 75 125
<br /> Copper(Cu),Dissolved 45.4 20 50 0 91 75 125
<br /> Arsenic(As),Dissolved 739 5 50 685.6 106 75 125
<br /> Molybdenum(Mo),Dissolved 126 5 50 81.4 89 75 125
<br /> Cadmium(Cd),Dissolved 45.5 2 50 0 91 75 125
<br /> Barium(Be),Dissolved 598 5 50 556.2 84 75 125
<br /> Mercury(Hg),Dissolved 0.9 1 1 0 90 75 125
<br /> Lead(Pb),Dissolved 45.4 5 50 0 91 75 125
<br /> Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method 200.8
<br /> File ID: 068_ Batch ID:32636 Analysis Date: 031215/20142115
<br /> Sample 10: 14031324-"AMSD Units: pg1L Run ID:ICPIMS_1140325C Prep Date: 03/2412014 15:43
<br /> Analyte Result PQL SpkVal SpkRefVal%REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual
<br /> Magnesium(Mg),Dissolved 64700 500 5000 59840 97 75 125 63650 1.5(20)
<br /> Calcium(Ca),Dissolved 123000 500 5000 118300 95 75 125 121700 1.2(20)
<br /> Chromium(Cr),Dissolved 64.6 10 50 15.5 98 75 125 627 3.0(20)
<br /> Manganese(Mri Dissolved 488 5 500 0 9B 75 125 462.3 5.5(20)
<br /> Nickel(Ni),Dissolved 46.8 10 50 0 94 75 125 46.1 1.6(20)
<br /> Copper(Cu),Dissolved 46.1 20 50 0 92 - 75 125 45.4 1.5(20)
<br /> Arsenic(As),Dissolved 737 5 50 685.6 103 75 125 738.6 0.2(20)
<br /> Molybdenum(Mo),Dissolved 129 5 50 81.4 94 75 125 126.1 1.9(20)
<br /> Cadmium(Cd),Dissolved 48.2 2 50 0 96 75 125 45.5 5.8(20)
<br /> Barium(Be),Dissolved 623 5 50 556.2 134 75 125 598.3 4.1(20) M3
<br /> Mercury Lead(Pb)HDissolved ed 46.8 5 50 0 94 75 125 45.4 3.0(20)
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