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Alpha Analytical, Inc. <br /> 255 Glendale Ave. -Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 27-Mm-14 QC Summary Report /4032043 <br /> Method Blank Type MBLK Test Code:EPA Method SW8015B/C/SW82608 <br /> File ID:C:IHPCHEM1MS101DATAH40325114032504,D Batch ID:MSIOW0325B Analysis Date: 03/251201410:24 <br /> Sample ID: MBLK MSIOW0325B Units: pg1L Run ID:MSD_10_140326A Prep Date: 0312&201410:24 <br /> Analyte Result PQL SpkVal SpkRefVal%REC LCL(ME) UCL(ME)RPDReNaI %RPD(Limit) Qual <br /> TPH-P(GRO) ND 50 <br /> Surr: 1,2-Dichloroethane-04 9.59 10 96 70 130 <br /> Surr:Toluene-d8 10.2 10 102 70 130 <br /> Surr.4-Bromolluorobenzene 9.62 10 96 70 130 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8015B/C I SW82608 <br /> File ID: C:IHPCHEM1MS101DATA\140325114032503.0 Batch ID:MS10W0326B Analysis Date: 031251201409:37 <br /> Sample ID: GLCS M310W0325B Units;pg/L Run 10:MSD 10_140325A Prep Date: 03125/2014 09:37 <br /> Analyte Result PQL SpkVal SpkRefVsl %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Unnit) Qual <br /> TPH-P(GRO) 405 50 400 101 70 130 <br /> Surr.1,2-Dichloroethane-d4 10.1 10 101 70 130 <br /> Surr:Toluene-d8 9.55 10 96 70 130 <br /> Surr:4-Bromo0uorobenzene 9.63 10 96 70 130 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015B/C/SW8260B <br /> File ID:C:IHPCHEM1MSIOIDATA1140325114032517.D Batch ID:MSIDWO325B Analysis Date: 03125/201415:05 <br /> Sample ID: 14032448-01AGS Units:pg/L Run ID:MSD_10_140325A Prep Date: 0 3/2 512 014 16:05 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDReNaI %RPD(Limit) Dual <br /> TPH-P(GRO) 2660 250 20D0 0 133 54 143 <br /> Sun:1,2-Dichloroethane-d4 50.1 50 100 70 130 <br /> Surr:Toluene-d8 47.3 50 95 70 130 <br /> Surr.4-Bromo0uorobenzene 49.5 50 99 70 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW801 SB/C I SW8260B <br /> File ID: C:IHPCHEMIMSI0IDATA114032Ml4032518.D Batch ID:MSIOW03258 Analysis Date: 03126/201415:26 <br /> Sample ID'. 14032448-01AGSD Units:pg/L Run 10�MSD_10_140325A Prep Date: 03/25/2014 15:26 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDReNaI %RPD(Llme) Qual <br /> TPH-P(GRO) 1760 250 2000 0 88 54 143 2659 40.8(23) R5 <br /> Surr: 1,2-Dichlorcethane[f4 49.1 50 98 70 130 <br /> Surr.Toluene-08 47.8 50 96 70 130 <br /> Surr:4-Bromo0uorobenzene 47.9 50 96 70 130 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly <br /> R5=MS/MSD RPD exceeded the Murmory control limit.Recovery met acceptance criteria <br /> Reported in micrograms per Liter,per client request. <br />