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CASTLE ANALYTICAL LABORATORY <br /> Environmentai Testing Services 2333 Shuttle Drive Atwater CA 95301 Phone (209) 384-2930 <br /> Certificate #2079 Fax (209) 384 1 507 <br /> Krazan &Associates, Inc Client Project ID 034-99039 Sampled 2 18-99 <br /> 215 W Dakota Avenue Reference Number 2062 Received 2-19-99 <br /> Clovis CA 93612 Sample Description Soil Extracted 2-22-99 <br /> Attu Bruce Myers Sample Prep/Analysis Method EPA 503018015M 8020 Analyzed 2-23 99 <br /> Lab Numbers 2062-6S 7S 8S 9S Reported 2-26-99 <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br /> WITH STEX DISTINCTION <br /> ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE 10 SAMPLE ID SAMPLE ID <br /> S-6 S-7 S-8 S9 <br /> (mg/kg) (mg/kg} (mg/kg) (mglkg) (mg/kg) <br /> MTBE 0 010 NO 45 NO 43 <br /> BENZENE 00050 NO 00065 NO NO <br /> TOLUENE 00050 NO 0 054 ND NO <br /> ETHYL BENZENE 00050 NO NO ND ND <br /> . TOTAL XYLENES 00050 NO 00065 NO NO <br /> GASOLINE RANGE 1 0 ND 24- NO 21* <br /> HYDROCARBONS <br /> Report Limit Multiplication Factor 1 1 1 1 <br /> Report Limit Multiplication Factor MTBE only 10 10 <br /> " Gas value due mainly to MTBE <br /> Surrogate % Recovery FID-967%l PID-964% FID-981%l PI0•961% FID-822%1 PID42 B% FID-757%t PID-724% <br /> Instrument ID VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br /> Anaiytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST APPROVED BY <br /> Clan J Cone Ja C Phillips <br /> aboratory Director <br />