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I <br /> w J <br /> CASTLE ANALYTICAL LABORATORY j <br /> Environmental Testing Services 2333 Shuttle drive, Atwater, CA 95301 Phone: (209) 384-2930 <br /> Certificate ;*2079 Fax: (209) 384-1507 <br /> Krazan &Associates, Inc. Client Project ID: 034-99039 "Sampled: 2-18-99 <br /> 215 W. Dakota Avenue Reference Number: 2D62 Received: 2-19-99 <br /> Clovis, CA 93612 Sample Description: Soil Extracted: 2-22-99 <br /> Attn: Bruce Myers Sample Prep/Analysi Method: EPA 503018015M, 8020 Analyzed: 2-23-99 <br /> Lab Numbers: 2062-6S, 7S, 8S, 9S Reported: 2-26-99 <br /> I <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br /> WITH BTEX DISTINCTION <br /> ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> S-6 S-7 S-8 S-9 <br /> (mg/kg) (mg/kg) mg/kgl (mglkg) (mg/kg) <br /> MTBE 0.010 ND 4.5 ND 4.3 <br /> BENZENE 0.0050 ND 0.0065 ND ND <br /> TOLUENE 0.0050 ND 0.054 ND ND <br /> ETHYL BENZENE 0.0050 ND ND NO ND <br /> TOTAL XYLENES 0.0050 ND 0.0055 ND ND <br /> GASOLINE RANGE 1.0 ND 2.4* ND 2.1" <br /> HYDROCARBONS <br /> Report Limit Multiplication Factor: 1 1 1 1 <br /> Report Limit Multiplication Factor MTBE only: 10 10 <br /> * Gas value due mainly to MTBE. <br /> Surrogate % Recovery: F10-86.7%1PID-98.4% FID 6.1%1 PID-96.1% FID-82.2%f Pl"2.9% FID-75.7%I PID-72.4% <br /> Instrument ID: VAR-GC1 AR-GC1 VAR-GC1 VAR-GC1 <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit = Reporting Limit x Report Limit Multiplication Factor <br /> ANALYST: ✓. AP ROVED BY: <br /> Clari J. Cone Ja C. Phillips <br /> aboratory Director <br />