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i Report Number 41309 QC Report Matrix Spikel Matrix Spike (Duplicate Date 12/16/2004 Project Name MEYER Project Number 3490 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit TPH as Diesel Blank <50 1000 1000 1150 1080 uglL M EPA 8015 1218104 115 108 5 57 70-130 25 1,1-Dichloroethane 41345-01 <0 50 400 400 420 41 2 uglL EPA 8260E 1218104 105 103 1 88 70-130 25 Benzene 41345-01 <0 50 400 400 41 1 408 ug/L. EPA 8260B 1218104 103 102 0 772 70-130 25 1,2-Dichloroethane 41345-01 <0 50 400 400 41 3 406 uglL EPA 8260B 12!8104 103 102 159 70-130 25 Tofuene 41345-01 <0 50 400 400 39 2 386 uglL EPA 8260E 1218104 981 965 167 70-130 25 Chlorobenzene 41345-01 <0 50 400 400 407 401 uglL EPA 82608 1218104 102 100 143 70-130 25 Tert-Butanol 41345-01 5300 200 200 5760 4520 uglL EPA 8260B 1218104 238 000 200 70-130 25 Methyl-t-Butyl Ether41345-01 890 400 400 895 888 uglL EPA 8260E 1218104 142 000 200 70-130 25 1,1-Dichloroethane 41451-01 <0 50 400 400 376 366 uglL EPA 8260E 12/13/04 940 91 6 250 70-130 25 Benzene 41451-01 <0 50 400 400 388 377 uglL EPA 826013 12/13/04 970 942 2 93 70-130 25 1,2-Dichloroethane 41451-01 <0 50 400 400 406 400 uglL EPA 8260E 12/13/04 102 100 151 70-130 25 Toluene 41451-01 <0 50 400 400 398 387 uglL EPA 82608 12/13/04 995 96 9 265 70-130 25 Chlorobenzene 41451-01 <0 50 400 400 394 388 uglL EPA 8260B 12/13/04 984 970 1 37 70-130 25 Tert-Butanol 41451-01 <50 200 200 199 198 ugfL EPA 8260B 12/13104 997 993 0 408 70-130 25 Methyl-t-Butyl Ether 41451-01 <0 50 400 400 356 351 uglL EPA 8260B 12/13/04 890 877 143 70-130 25 Approved By Jo iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-2974800