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• i • Report!Number 41317 QC Report Matrix Spike/Matrix Spike Duplicate Date 12/1312004 Project Name CASSIDY Project Number 3490 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample_ Value Level Level Value Value Units Method Analyzed Recov Recov_ Diff Limit - Limit TPM as Diesel Blank <50 1000 1000 987 1070 ug/L M EPA 8015 1217104 987 107 803 70-130 25 1,1-Dichloroethane 41345-01 <0 50 400 400 420 41 2 ug/L EPA 8260E 1218104 105 103 1 88 70-130 25 Benzene 41345-01 <0 50 400 400 41 1 408 uq/L EPA 82608 1218104 103 102 0 772 70-130 25 1,2-Dichloroethane 41345-01 <0 50 400 400 41 3 406 ug/L EPA 82608 1218104 103 102 159 70-130 25 Toluene 41345-01 <0 50 400 400 392 386 ug/L EPA 8260B 1218104 981 965 1 67 70-130 25 Chlorobenzene 41345-01 <0 50 400 400 407 401 ug/L EPA 8260E 12/8104 102 100 143 70-130 25 Tert-Butanol 49345-01 5300 200 200 5760 4520 ug/L EPA 82608 1218/04 238 000 200 70-130 25 Methyl-t-Butyl Ether 41345-01 890 400 400 895 888 ug/L EPA 8260E 1218104 142 000 200 70-130 25 1,1-Dichloroethane 41402-01 <0 50 400 400 367 352 ug/L EPA 8260E 12/11/04 917 879 423 70-130 25 Benzene 41402-01 <0 50 400 400 389 377 ug/L EPA 8260E 12/11/04 973 94 2 324 70-130 25 1 2-Dichloroethane 41402-01 <0 50 400 400 41 1 405 ug/L EPA 82608 12/11/04 103 101 144 70-130 25 Toluene 41402-01 <0 50 400 400 409 394 ug/L EPA 8260B 12/11104 102 98 5 371 70-130 25 Chlorobenzene 41402-01 <0 50 400 400 397 384 ug1L EPA 8260E 12/11/04 994 961 330 70-130 25 Tert-Butanol 41402-01 <5 0 200 200 203 201 ug/L EPA 8260E 12/11/04 102 101 0 993 70-130 25 Methyl-t-Butyl Ether41402-01 <0 50 400 400 350 348 ug/L EPA 8260B 12/11/04 875 869 0 751 70-130 25 Approved By ,toe Iff KIFF ANALYTICAL, LLC 2795 2nd St Suite 300 Davis, CA 95616 530-297-4800