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i Report Number 41314 QC Report Matrix Spike/Matrix Spike Duplicate Date 12/13/2004 Project Name Robles Project Number 3490 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike DUD Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit TPH as Diesel Blank <50 1000 1000 1150 1080 ug/L M EPA 8015 1218104 115 108 557 70-130 25 1,1-Dichloroethane 41314-01 <0 50 400 400 377 383 ug/L EPA 82603 1218104 943 958 160 70-130 25 Benzene 41314-01 <0 50 400 400 403 410 ug/L EPA 8260E 1218104 101 102 1 70 70-130 25 1,2-Dichloroethane 41314-01 <0 50 400 400 400 404 ug/L EPA 8260B 12!8104 999 101 1 15 70-130 25 Toluene 41314-01 <0 50 400 400 399 403 ug/L EPA 82606 1218104 998 101 0 856 70-130 25 Chlorobenzene 41314-01 <0 50 400 400 401 406 ug/L EPA 82608 1218104 100 101 1 10 70-130 25 Tert-Butanol 41314-01 <5 0 200 200 191 192 ug/L EPA 8260E 1218104 957 961 0 413 70-130 25 Methyl-t-Butyl Ether41314-01 1 8 400 400 432 442 ug/L EPA 8260B 1218104 103 106 224 70-130 25 1,1-Dichloroethane 41368-01 <0 50 400 400 376 361 ug/L. EPA 8260B 1219104 940 903 400 70-130 25 Benzene 41368-01 24 400 400 429 41 9 ug/L EPA 8260B 1219/04 101 987 252 70-130 25 1,2-Dichloroethane 41368-01 <0 50 400 400 388 387 ug/L EPA 8260E 1219104 971 968 0 367 70-130 25 Toluene 41368-01 <0 50 400 400 399 389 ug/L EPA 82606 1219104 998 974 250 70-130 25 Chlorobenzene 41368-01 <0 50 400 400 403 393 ug/L EPA 8260E 12/9104 101 983 248 70-130 25 Tert-Butanol 41368-01 <5 0 200 200 193 187 ug/L EPA 8260E 1219104 966 936 318 70-130 25 Methyl-t-Butyl Ether 41368-01 71 400 400 461 463 ug/L EPA 82606 1219104 974 98 0 0 642 70-130 25 I y KIFF ANALYTICAL, LLC Approved By Joe iff 2795 2nd St, Suite 300 Davis, CA 95616 530-2974800