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Report Number 41307 QC Report Matrix Spike/Matrix Spike Duplicate Date 12/13/2004 Project Name MACK Project Number 3490 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit TPH as Diesel Blank <50 1000 1000 906 978 ug/L M EPA 8015 1218104 906 978 764 70-130 25 1,1-Dichloroethane 41345-01 <0 50 400 400 420 41 2 ug/L EPA 8260B 1218104 105 103 1 88 70-130 25 Benzene 41345-01 <0 50 400 400 41 1 408 ug1L EPA 82606 1218!04 103 102 0 772 70-130 25 1,2-Dichloroethane 41345-01 <0 50 400 400 41 3 406 ug1L EPA 8260E 1218104 103 102 1 59 70-130 25 Toluene 41345-01 <0 50 400 400 39 2 38 6 ug/L. EPA 8260B 1218104 981 965 1 67 70-130 25 Chlorobenzene 41345-01 <0 50 400 400 407 401 ug1L EPA 8260B 1218104 102 100 143 70-130 25 Tert-Butanol 41345-01 5300 200 200 5760 4520 ug/L EPA 8260B 1218104 238 000 200 70-130 25 Methyl-t-Butyl Ether41345-01 890 400 400 895 888 ug/L EPA 82606 1218104 142 000 200 70-130 25 1,1-Dichloroethane 41350-02 <0 50 400 400 375 363 ug/L EPA 8260B 1219104 938 907 332 70-130 25 Benzene 41350-02 <0 50 400 400 385 376 ug/L EPA 8260B 1219104 963 941 2 35 70-130 25 1,2-Dichloroethane 41350-02 <0 50 400 400 406 400 ug1L EPA 8260B 1219104 102 100 150 70-130 25 Toluene 41350-02 <0 50 400 400 400 393 ug1L EPA 8260B 1219104 100 983 175 70-130 25 Chlorobenzene 41350-02 <0 50 400 400 389 382 ug/L EPA 8260B 1219104 973 954 1 97 70-130 25 Tert-Butanol 41350-02 13 200 200 208 208 ug1L EPA 8260B 1219104 975 974 00553 70-130 25 Methyl-t-Butyl Ether 41350-02 <0 50 400 400 358 352 ug/L EPA 8260B 1219104 89 5 88 0 164 70-130 25 i Approved By ,!o iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800