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S Report Number 41312 QC Report Matrix Spike/Matrix Spike Duplicate Date 12113/2004 Project Name WILSON Project Number 3490 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked 5ppked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Anal zed Recov Recov Diff Limit Limit TPH as Diesel Blank <50 1000 1000 1150 1080 ug/L M EPA 8015 1218104 115 108 557 70-130 25 1 1-Dichloroethane 41314-01 <0 50 400 400 377 383 ug/L EPA 8260B 1218104 943 958 1 60 70-130 25 Benzene 41314-01 <0 50 400 400 403 410 ug/L EPA 8260E 1218104 101 102 1 70 70-130 25 1,2-Dichloroethane 41314-01 <0 50 400 400 400 404 ug/L EPA 8260B 12/8104 999 101 1 15 70-130 25 Toluene 41314-01 <0 50 400 400 39 9 403 ug/L EPA 82608 1218104 998 101 0 856 70-130 25 Chlorobenzene 41314-01 <0 50 400 400 401 406 ug/t EPA 82606 1218104 100 101 1 10 70-130 25 Tert-Butanol 41314-01 <5 0 200 200 191 192 ug/L. EPA 8260B 12!8104 95 7 961 0 413 70-130 25 Methyl-t-Butyl Ether41314-01 1 8 400 400 432 442 ug/L EPA 8260E 1218104 103 106 224 70-130 25 1,1-Dichloroethane 41368-01 <0 50 400 400 376 361 ug/L EPA 8260B 1219!04 940 903 400 70-130 25 Benzene 41368-01 24 400 400 429 419 ug/L EPA 8260B 1219104 101 987 2 52 70-130 25 1,2-Dichloroethane 41368-01 <0 50 400 400 388 387 ug/L EPA 8260B 1219!04 971 968 0 367 70-130 25 Toluene 41368-01 <0 50 400 400 399 389 ug/L EPA 8260E 1219!04 998 974 250 70-130 25 Chlorobenzene 41368-01 <0 50 400 400 403 393 ug1L EPA 8260E 1219104 101 983 248 70-130 25 Ter(-Butanol 41368-01 <5 0 200 200 193 187 ug/L EPA 8260B 1219104 966 936 318 70-130 25 Methyl-t-Butyl Ether41368-01 71 400 400 461 463 ug/L EPA 82606 1219104 974 980 0 642 70-130 25 Approved By Jo iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800