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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 4 <br /> http l/www mccampbell� E-mail main@mccampbell com <br /> Inc Client Project ID Frank's One Stop Date Sampled 06/10/98 <br /> [Remedy, <br /> 12 Dove Court Date Received 06/10/99 <br /> Vacaville,CA 95687 Client Contact Paul LeCheminant Dare Extracted 06/10/98 <br />' Chent P O Date Analyzed 06/10-06/11/98 <br /> EPA method 8260 Volatile Organics By GUMS <br /> Lab ID 90310 <br /> Client ID PL-0610-1 <br /> Matrix S <br /> Compound Concentration` Compound Concentration* <br /> Acetone ND<35 Ethyibenzene 42 <br /> Benzene 65 Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br />' Bromochloromethane ND isopropy[benzene ND <br /> Bromodichloromethane ND p-isopropyl toluene ND <br /> Bromoform I ND Methyl butyl ketone ND <br /> Bromomethane ND Methyiene Ch[onde` ND <br />' n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Butyl benzene ND Methyl isobutyl ketones ND <br /> tart-Butyl benzene 84 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Naphthalene I I <br /> Carbon Tetrachloride ND n-Propyl benzene t4 <br /> Chlorobenzene ND StyreneND <br /> Chloroethane ND III 12-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ethe ND 1 1,2 2-Tetrachloroethane ND <br />' Chloroform ND Tetrachloroethane ND <br /> F4-Chlorotoluene <br /> oromethane ND Toluene 90 <br /> hlorotoluene ND 12,3-Tnchlorobenzene ND <br /> ND l,2 4-Tnchlorobenzene ND <br /> omochloromethane ND 1 I,l-TnchloroethaneND <br /> Dibromo-3-chlompropane ND III 2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br />' l 2-Dichlorobenzene ND I nchlorotluoromethane ND <br /> pmpane <br /> 1,3-Dichlorobenzene ND 1,2,3-TnchloroND <br /> 1,4-Dichlorobenzene ND 1,24-Tnmethylbenzene 62 <br /> Dichlorodifluoromethane ND 13,5-Tnmethylbenzene 10 <br /> I <br /> 1,1-Dichloroethane ND Vinyl Acetate ` ND <br /> 12-Dich[oroethane ND Vinyl Chlonde "' ND <br /> 1 1-Dichloroethene ND Xylenes total 220 <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> l 2-Dichloropropane ND <br /> i 3-Dichlotopropane ND <br /> 2 2-Dichloropropane ND Comments <br />�i <br /> IJ-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromotluoromethane 109 <br /> trans-l3-Dichloropropene I ND Toluene-d8 95 <br /> Ethylene dibromide ND 4-Bromotluorobenzene 92 <br /> I water and vapor samples are reported in ug/L,sod and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (1) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 i Edward Hamilton, Lab Director <br />