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QC Sample Results <br /> Client: Veolia Environmental Services Job ID: 720-95524-1 <br /> Project/Site: Stockton Logistics-Stockton, CA <br /> Method: 82608 -Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCS 440-575397/2-A Client Sample ID: Lab Control Sample <br /> Matrix: Water Prep Type: TCLP <br /> Analysis Batch: 575736 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Bromomethane 0.100 0.108 mg/L 108 64-139 <br /> Carbon tetrachloride 0.100 0.108 mg/L 108 60-150 <br /> Chlorobenzene 0.100 0.107 mg/L 107 70-130 <br /> Chloroethane 0.100 0.120 mg/L 120 64-135 <br /> Chloroform 0.100 0.109 mg/L 109 70-130 <br /> Chloromethane 0.100 0.167 mg/L 167 47-140 <br /> cis-1,2-Dichloroethene 0.100 0.115 mg/L 115 70-133 <br /> cis-1,3-Dichloropropene 0.100 0.105 mg/L 105 70-133 <br /> Dibromomethane 0.100 0.117 mg/L 117 70-130 <br /> Dichlorodifluoromethane 0.100 0.104 mg/L 104 29-150 <br /> Ethylbenzene 0.100 0.104 mg/L 104 70-130 <br /> - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - <br /> Hexachlorobutadiene 0.100 0.0995 mg/L 100 10-150 <br /> Isopropylbenzene 0.100 0.103 mg/L 103 70-136 <br /> m,p-Xylene 0.100 0.0970 mg/L 97 70-130 <br /> Methylene Chloride 0.100 0.133 * mg/L 133 52-130 <br /> Naphthalene 0.100 0.104 mg/L 104 60-140 <br /> n-Butylbenzene 0.100 0.104 mg/L 104 65-150 <br /> N-Propylbenzene 0.100 0.0987 mg/L 99 67-139 m <br /> o-Xylene 0.100 0.110 mg/L 110 70-130 <br /> sec-Butyl benzene 0.100 0.102 mg/L 102 70-138 <br /> Styrene 0.100 0.0912 mg/L 91 70-134 <br /> tert-Butyl benzene 0.100 0.0936 mg/L 94 70-130 <br /> Tetrachloroethene 0.100 0.102 mg/L 102 70-130 <br /> Toluene 0.100 0.109 mg/L 109 70-130 <br /> trans-1,2-Dichloroethene 0.100 0.111 mg/L 111 70-130 <br /> trans-1,3-Dichloropropene 0.100 0.100 mg/L 100 70-132 <br /> Trichloroethene 0.100 0.115 mg/L 115 70-130 <br /> Trichlorofluoromethane 0.100 0.114 mg/L 114 60-150 <br /> Vinyl chloride 0.100 0.140 mg/L 140 59-133 <br /> 1,2-Dibromoethane(EDB) 0.100 0.108 mg/L 108 70-130 <br /> Bromochloromethane 0.100 0.116 mg/L 116 70-130 <br /> Bromodichloromethane 0.100 0.117 mg/L 117 70-132 <br /> Dibromochloromethane 0.100 0.109 mg/L 109 69-145 <br /> p-Isopropyltoluene 0.100 0.107 mg/L 107 70-132 <br /> 2-Butanone(MEK) 0.500 0.669 mg/L 134 44-150 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 101 80-128 <br /> 4-Bromofluorobenzene(Surr) 91 80-120 <br /> Dibromofluoromethane(Surr) 103 76-132 <br /> Lab Sample ID: 720-95524-1 MS Client Sample ID: 100419 A <br /> Matrix: Water Prep Type: TCLP <br /> Analysis Batch: 575736 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,1,1-Trichloroethane ND 0.100 0.106 mg/L 106 70-130 <br /> 1,1,2,2-Tetrachloroethane ND 0.100 0.127 mg/L 127 63-130 <br /> Eurofins TestAmerica, Pleasanton <br /> Page 10 of 29 10/28/2019 (Rev. 1) <br />