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QC Sample Results <br /> Client: Veolia Environmental Services Job ID: 720-95524-1 <br /> Project/Site: Stockton Logistics-Stockton, CA <br /> Method: 82608 -Volatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: 720-95524-1 MS Client Sample ID: 100419 A <br /> Matrix: Water Prep Type: TCLP <br /> Analysis Batch: 575736 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Trichlorofluoromethane ND 0.100 0.112 mg/L 112 6O__15-0 <br /> Vinyl chloride ND F1 0.100 0.143 F1 mg/L 143 50-137 <br /> 1,2-Dibromoethane(EDB) ND 0.100 0.115 mg/L 115 70-131 <br /> Bromochloromethane ND 0.100 0.112 mg/L 112 70-130 <br /> Bromodichloromethane ND 0.100 0.118 mg/L 118 70-138 <br /> Dibromochloromethane ND 0.100 0.106 mg/L 106 70-148 <br /> p-Isopropyltoluene ND 0.100 0.106 mg/L 106 70-130 <br /> 2-Butanone(MEK) 0.11 0.500 0.802 mg/L 139 48-140 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> Toluene-d8(Surr) 104 80-128 <br /> 4-Bromofluorobenzene(Surr) 92 80-120 <br /> Dibromofluoromethane(Surr) 103 76-132 <br /> Lab Sample ID: 720-95524-1 MSD Client Sample ID: 100419 A <br /> Matrix: Water Prep Type: TCLP <br /> Analysis Batch: 575736 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1,1,2-Tetrachloroethane ND 0.100 0.105 mg/L 105 60-149 4 20 <br /> 1,1,1-Trichloroethane ND 0.100 0.108 mg/L 108 70-130 2 20 <br /> 1,1,2,2-Tetrachloroethane ND 0.100 0.119 mg/L 119 63-130 6 30 <br /> 1,1,2-Trichloroethane ND 0.100 0.107 mg/L 107 70-130 4 25 <br /> 1,1-Dichloroethane ND F1 " 0.100 0.137 F1 mg/L 137 65-130 1 20 <br /> 1,1-Dichloroethene ND 0.100 0.104 mg/L 104 70-130 1 20 <br /> 1,1-Dichloropropene ND 0.100 0.115 mg/L 115 64-130 2 20 <br /> 1,2,3-Trichlorobenzene ND 0.100 0.107 mg/L 107 60-140 1 20 <br /> 1,2,3-Trichloropropane ND 0.100 0.114 mg/L 114 60-130 3 30 <br /> 1,2,4-Trichlorobenzene ND 0.100 0.109 mg/L 109 60-140 2 20 <br /> 1,2,4-Trimethylbenzene ND 0.100 0.0965 mg/L 96 70-130 2 25 <br /> 1,2-Dibromo-3-Chloropropane ND 0.100 0.0992 mg/L 99 48-140 10 30 <br /> 1,2-Dichlorobenzene ND 0.100 0.109 mg/L 109 70-130 2 20 <br /> 1,2-Dichloroethane ND 0.100 0.119 mg/L 119 56-146 5 20 <br /> 1,2-Dichloropropane ND F1 0.100 0.147 F1 mg/L 147 69-130 2 20 <br /> 1,3,5-Trimethylbenzene ND 0.100 0.0978 mg/L 98 70-130 2 20 <br /> 1,3-Dichlorobenzene ND 0.100 0.110 mg/L 110 70-130 1 20 <br /> 1,3-Dichloropropane ND 0.100 0.121 mg/L 121 70-130 3 25 <br /> 1,4-Dichlorobenzene ND 0.100 0.104 mg/L 104 70-130 0 20 <br /> 2,2-Dichloropropane ND 0.100 0.111 mg/L 111 69-138 1 25 <br /> 2-Chlorotoluene ND 0.100 0.100 mg/L 100 70-130 1 20 <br /> 4-Chlorotoluene ND 0.100 0.0973 mg/L 97 70-130 1 20 <br /> Benzene ND 0.100 0.124 mg/L 124 66-130 1 20 <br /> Bromobenzene ND 0.100 0.0981 mg/L 98 70-130 2 20 <br /> Bromoform ND 0.100 0.0986 mg/L 99 59-150 1 25 <br /> Bromomethane ND 0.100 0.110 mg/L 110 62.131 5 25 <br /> Carbon tetrachloride ND 0.100 0.108 mg/L 108 60-150 1 25 <br /> Chlorobenzene ND 0.100 0.109 mg/L 109 70-130 2 20 <br /> Chloroethane ND 0.100 0.122 mg/L 122 68-130 4 25 <br /> Eurofins TestAmerica, Pleasanton <br /> Page 12 of 29 10/28/2019 (Rev. 1) <br />