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S U R R Q G A T E R E C O V E R I E S R E P O R T Job Number 200207 Report Date 02/03/2000 ' CUSTOMER IT Group PROJECT Southland - Martinez ATTN Rhonda Teicheira Method Volatile Organics -Aromatics Batch 10817 Method Code 8020BX Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time MB 1 53 47 50 0000 106 9 64-147 01/28/2000 1053 LCS 1 55 61 50 0000 111 2 64-147 01/28/2000 1211 LCD 1 56 01 50 0000 112 0 64-147 01/28/2000 1236 200162-2 Liquids 25 47 68 50 0000 95 4 64-147 01/28/2000 1537 200135-13 Liquids 10 47 58 50 0000 95 2 64-147 01/28/2000 1603 200135-14 Liquids 25 48 62 50 0000 97 2 64-147 01/28/2000 1629 200202-1 Liquids 1 47 44 50 0000 94 9 64-147 01/28/2000 1654 ' 200206-1 Liquids 1 47 44 50 0000 94 9 64-147 01/28/2000 1720 200206-2 Liquids 1 47 59 50 0000 95.2 64-147 01/28/2000 1746 200206-3 Liquids 1 47 27 50 0000 94 5 64-147 01/28/2000 1812 06-4 Liquids 1 47 78 50 DD00 95 6 64-147 01/28/2000 1837 1406-5 Liquids 1 47 14 50 0000 94 3 64-147 01/28/2000 1903 06-6 Liquids 1 47.96 50 0000 95 9 64-147 01/28/2000 1929 200207-1 Liquids 1 46 85 50 0000 93 7 64-147 01/28/2000 2137 200207-3 Liquids 1 46 87 50 0000 93 7 64-147 01/28/2000 2229 200208-1 Liquids 1 44 45 50 0000 88 9 64-147 01/28/2000 2254 200208-2 Liquids 1 44 37 50 0000 88 7 64-147 01/28/2000 2320 200208-3 Liquids 1 46 75 50 0000 93 5 64-147 01/28/2000 2346 200206-5 Liquids MS 1 47 62 50 0000 95 2 64-147 01/29/2000 0219 200206-5 Liquids MSD 1 48 09 50 0000 96 2 64-147 01/29/2000 0245 Method Volatile Organics Aromatics Batch 10847 Method Code 8020BX Analyst evd ' Surrogate Units 4-Bromofluorobenzene ug/L Lab 10 Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time MB 1 43 98 50 0000 88 0 64-147 01/31/2000 1213 ' 200190-6 Liquids 1 47 17 50 0000 94 3 64-147 01/31/2000 1240 1 200197-1 Solid 50000 56 77 50 0000 113 5 64-147 01/31/2000 1306 LCS 1 44 28 50 0000 88 6 64-147 01/31/2000 1452 LCD 1 43 59 50 0000 87 2 64-147 01/31/2000 1518 1 200207-1 Liquids 5 43 42 50 0000 86 8 64-147 01/31/2000 1544 200207-2 Liquids 1 43 01 50 0000 86 0 64-147 01/31/2000 1610 200226-5 Solid 1 43 49 50 0000 87 0 64-147 01/31/2000 1637 200225-1 Solid 1 44 18 50 0000 88 4 64-147 01/31/2000 1703 200225-2 Solid 1 43 96 50 0000 87 9 64-147 01/31/2000 1729 200225-3 Solid 1 43 40 50 0000 86 8 64-147 01/31/2000 1756 25-4 Solid 1 43 44 50 0000 86 9 64-147 01/31/2000 1822 25-5 Solid 1 43 60 50 0000 87 2 64-147 01/31/2000 2032 225-6 Solid 1 43 04 50 0000 86 1 64-147 01/31/2000 2058 200225-7 Solid 1 44 98 50 0000 90 0 64-147 01/31/2000 2124 Page 11