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(OfiLAB CORE LABORATORIES <br /> S U R R 0 G A T E R E C O V E R I E S R E P O R T <br /> Job Number 991123 Report Date 06/30/1999 <br /> CUSTOMER IT Group PROJECT: Southland - Martinez ATTN Shelby Lathrop <br /> Method Volatile Organics by GC/MS Batch 6870 <br /> Method Code 82600x Analyst gfb <br /> Surrogate Units <br /> Dibromofluoromethane ug/L <br /> Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time <br /> 990876-23 Solid 1 31 66 25 000 126 6 60-160 05/24/1999 1052 <br /> 090876-23 Solid MS 22 26 25 000 89 0 60-160 05/24/1999 1411 <br /> 90876-23 Solid MSD 25 24 25 000 101 0 60-160 05/24/1999 1440 <br /> 90881-3 Liquids 1 30 04 25 000 120 2 57-162 05/25/1999 1102 <br /> 90881-3 Liquids MS 27 33 25 000 109 3 57-162 05/25/1999 1130 <br /> 990881-3 Liquids MSD 29 31 25 000 117 2 57-162 05/25/1999 1159 <br /> MB 1 25 76 25 000 103 0 57-162 06/22/1999 1516 <br /> LCS 1 24 75 25 000 99 0 57-162 06/22/1999 1618 <br /> 191123-6 Liquids 1 24 88 25 000 99 5 57-162 06/22/1999 1647 <br /> 991123-7 Liquids 1 26 82 25 000 107 3 57-162 06/22/1999 1715 <br /> 0&23-9 Liquids 1 25 74 25 000 103 0 57-162 06/22/1999 1812 { <br /> 3-10 Liquids 1 24 49 25 000 98 0 57-162 06/22/1999 1841 �V <br /> 4-10 Liquids 1 26 69 25 000 106 8 57-162 06/22/1999 1909 <br /> 91124-9 Liquids 1 25 90 25 000 103 6 57-162 06/22/1999 1938 <br /> 991124-8 Liquids 10 25 27 25 000 101 1 57-162 06/22/1999 2006 <br /> 91124-7 Liquids 1 26 61 25 000 106 4 57-162 06/22/1999 2035 <br /> 91124-6 Liquids 1 27 76 25 000 111 0 57-162 06/22/1999 2103 <br /> 91124-5 Solid 1 24 33 25 000 97 3 60-160 06/22/1999 2132 <br /> 991124-4 Solid 1 25 81 25 000 103 2 60-160 06/22/1999 2201 <br /> 91124-3 Solid 1 24 95 25 000 99 8 60-160 06/22/1999 2229 <br /> 91124-2 Solid 1 24 09 25 000 96 4 60-160 06/22/1999 2258 <br /> 91124-1 Solid 1 25 56 25 000 102 2 60-160 06/22/1999 2327 <br /> 91123-1 Solid 1 25 12 25 000 100 5 60-160 06/22/1999 2355 <br /> 991123-2 Solid 1 23 18 25 000 92 7 60-160 06/23/1999 0024 <br /> 91123-3 Solid 1 25 12 25 000 100 5 60-160 06/23/1999 0053 <br /> 91123-4 Solid 1 24 83 25 000 99 3 60-160 06/23/1999 0122 <br /> 91123-5 Solid 1 25 69 25 000 102 8 60-160 06/23/1999 0150 <br /> Method Volatile Organics by GC/MS Batch 6885 <br /> Method Code 8260OX Analyst gfb <br /> Surrogate Units <br /> Dtbromofluoromethane ug/L <br /> Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time <br /> 90881-3 Liquids 1 30 04 25 000 120 2 57-162 05/25/1999 1102 <br /> 990881-3 Liquids MS 27 33 25 000 109 3 57-162 05/25/1999 1130 <br /> 90881-3 Liquids MSD 29 31 25 000 117 2 57-162 05/25/1999 1159 <br /> LCS 1 24 20 25 000 96 8 57-162 06/23/1999 1049 <br /> MB 1 23 94 25 000 95 8 57-162 06/23/1999 1118 <br /> 3-8 Liquids 200 23 26 25 000 93 0 57-162 06/23/1999 1146 <br /> 5-3 Solid 1 24 28 25 000 97 1 60-160 06/23/1999 1312 <br /> 91125-9 Solid 1 24 35 25 000 97 4 60-160 06/23/1999 1604 <br /> Page 22 <br /> TI arahlKal esWla ounlona IX wiyryretafona Mnlam04 ul Ilya rep«1 are basa6—n nl ormaLon IN*t1e11 W—11 aclusrve eM cont tlenl al LSe tly9 ap«l lie been maga^lo arNlyla3'resWte cancans«wtarpe{a Lona <br /> expre5Sa0 ret•nse�l Ine best WaOmenl pl Cde Leb«etpr Is Carr Labaelwres Iwweva rra4ea na wa s ly a awayematwn q o ass or—'p of.y rypa antl e p esaly d ecla me same ea tO Ine wop c*rvlty pope opera oma a pral Iabl.n of <br /> any al yes('pal 0 ulna In neral p pearly we11«aaM m cpnneclOn vnm can h wGn eit016 p590 w 8f ed Wnn hr amy realm wMtSoavar This report an all rwt be ePOtlaCeO n Mwla or n par w ul Ine ynaten app—1 nl CO Lahprelpn¢s <br />