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CORLA-8 CORE LABORATORIES 0 U A L I T Y A S S U R A N C E F 0 0 T E R METHOD REFERENCES (1) EPA SW-846, Test Methods for Evaluating Solid waste, Third Edition, September 1986, and Updates 1, I1, IIA, IIB, and III (2) Standard Methods for the Examination of Water and Wastewater, 18th Edition, 1995 (3) EPA 600/4-79-020, Methods of Chemical Analysts for Waters and Wastes, March 1983 (4) Federal Register, Friday, October 26, 1984 (40 CFR Part 136) and amendments (5) American Society for Testing and Materials, Volumes 5.01, 5 02, 5 03, 1992 (6) EPA 600/4-89-001, Short-term Methods for Estimating the Chronic Toxicity of Effluents and Receiving Waters to Fresh Water Organisms (7) EPA 600/4-90-027, Methods for Measuring the Acute Toxicity of Effluent and Receiving Waters to Fresh Water and Marine Organisms, Fourth Edition COMMENTS All methods of chemical analysis have a statistical uncertainty associated with the results Unless otherwise indicated, the data in this report are within the Limits of uncertainty as specified in the referenced method Quality control acceptance criteria are based either on Limits specified in the referenced method or on actual Laboratory performance. The date and time of analysis indicated on the report may not reflect the actual time of analysis for QC samples Data reported in the QC report may be Lower than sample data due to dilution of samples into the calibration range of the anatysis Sample concentrations for solid samples are calculated on an as received (wet) basis unless otherwise indicated Unless otherwise indicated, volatites by gas chromatography (GC) are reported from a single Colum Volatiles analyses by GC on low level soils are conducted at room temperature TCLP extractions are performed at sample amounts, approved by the state of California FLAGS, FOOTNOTES, AND ABBREVIATIONS (as needed) = Not analyzed N I. = Not Ignitable N/A = Not applicable S I. = Sustains Ignition ug/L = Micrograms per liter I(HS) = Ignites, but does not Sustain ignition mg/L = Milligrams per liter RPD = Relative Percent Difference ND = Not detected at a value greater than the reporting limit NC = Not calculable due to values lower than the detection limit (a) = Surrogate recoveries were outside QC Limits to due matrix effects. {b) = Surrogate recoveries were not calculated due to dilution of the sample below the detectable range for the surrogate. (c) = Matrix spike recoveries were outside QC Limits due to matrix effects (d) = Relative Percent Difference (RPD) for duplicate analysis outside OC limits due to actuat differences in the sampte matrix. (e) = The limit Listed for flammability indicates the upper limit for the test SampLes are not tested at temperatures above 140 Fahrenheit since only saaples which will sustain ignition at temperatures below 140 are considered f laffeabte. (f) = Results for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quantified using a diesel standard, however, the hydrocarbon pattern did not match a diesel pattern (g) = ResuLts for this hydrocarbon range did not match a typical hydrocarbon pattern. Results were quantified using a gasoline standard, however, the hydrocarbon pattern did not match a gasoline pattern (h) = High dilution due to matrix effects QC SAMPLE IDEYTIcICATIONS SUBCONTRACTED LABORATORY LOCATIONS me = Method Stank SB = Storage Blank Core Laboratories Aurora, Colorado *AU RS = Reagent Stank MS = Matrix Spike Casper, Wyoming *CA ICS s Initigl Catibration Blank MSD = Matrix Spike Duplicate Carson, California *CP CCB = Continuing Calibration Blank MD = Matrix Duplicate Corpus Christi, Texas *CC CS = Calibration Standard SS = Blank Spike Edison, New Jersey *ED ICY = :nitiat Calibration SS = Surrogate Spike Houston, Texas (Env) *HE Verification LCS = Laboratory Control Houston, Texas (Pet) *HP CCY = Continuing Calibration Standard Indianapolis, Indiana *IN Verification RS = Reference Standard Lake Charles, Louisiana *LC Valparaiso, Indiana *VP Bakersfield, California *BK N1250 Gene Autry Way Autry Way ' Anaheim, CA 92W5 (714) 937-1094 /u/matt/togs_n_for=/footer.form ehn analYhcal esurcs.--.ar t.0.tahwts confalnad w�si ec pat a e bases—na}Orma and mala almpphad by the N"I for wlpae eecWs a xl wnrbant atss� ns r 1 has boon made Tho.maIy,[af to J1.ognlO dr nl0rp ata t o s ssea apl0sei l the bast ludo mei I of Caa Latwra[ s CMe Lado Id-holve makes r wa anty or apesuntaho Sep ess a SIM ed of any tri a and e o ry d5 ll h e se me.ss to the prd Wfilty Mope opalelw b,p ChMblenass al any M Q..coil o o al n party—11 0 I-n .1R wf ch sooh repo t s wed or W Id u n lot ary—so +Aietsoa w Tlns repo f sh ill not ba a �C ..I.o oa I wphoul lira w am eW wet of Cas LabMa10 es