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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' hyp//www mccampbell com E-mail main@mccampbell com <br /> ' Advanced GeoEnvironmental Client Project ID Ram Water Carwash Date Sampled 04/30/01 <br /> 837 Shaw Road Date Received 05/01/01 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 05102-05/04/01 <br /> Client P O Date Analyzed 05/02-05/04/01 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 66596 <br /> ' Client ID MWl/043001 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Cancmtrauon* Repor'ng i tmlt <br /> ' W S W S <br /> Acetone ND<500 50 25 trans-1,3-Dtehloropropene ND<500 1 0 50 <br /> Benzene ND<500 10 50 Ethylene dibminide ND<500 10 50 <br /> Bromobenzene ND<500 10 5 0 Ethylbenzene ND<500 10 5 0 <br /> ' Bronwehloromethane ND<500 to 5 0 Hexachlorobutadiene ND<500 50 25 <br /> Brornodichloromethane ND<500 10 50 lodomethane ND<500 10 50 <br /> Bromoform ND<500 10 5 0 Isopropylbenzene ND<500 10 5 0 <br /> Bromomethane ND<500 10 5 0 p-Isopropyl toluene ND<500 1 0 50 <br /> n-Butyl benzene - N13<500 1 0 5 0 Methyi butyl ketone ' ND<500 10 5 0 <br /> sec-Butyl benzene ND<500 1 0 5 0 Methylene Chlonde" ND<500 1 0 5 0 <br /> tent-Butyl benzene ND<500 10 50 Methyl ethyl ketone' ND<500 2 0H10Carbon Disulfide ND<500 10 50 Methyl isobutyl ketone ° ND<500 l0Carbon Tetrachlondt. ND<500 10 5 0 Methyl tert-Butyl Ether(MTBh) — 1 0Chlorobenzene ND<500 10 50Naphthalene ND<506 50 <br /> Chloroethane ND<500 1 0 50 n-Propyl benzene ND<5001{) 5 0 <br /> 2-Chloroethyl Vinyl L-thE ` ND<500 1 0 50 Styrene ND<500 l U 5 0 <br /> ' Chloroform 1400 10 50 1,11,2-Tetrachloroethane ND<500 10 50 <br /> Chloromethane ND<500 10 5 0 1 1,2,2-Tetrachloroethane ND0<500 1 5 0 <br /> 2-Chlorotoluene ND<500 10 5 0 Tetrachioroethene ND<500 E50 <br /> 5 0 <br /> 4-Chlorotoluene ND<500 10 5 0 Toluene ND<500 5 0 <br /> Dibromochloromethane ND<500 10 5 0 1,2,3-Tnchlorobenzene ND<500 25 <br /> 1,2-Dibromo-3-chioropropane ND<500 20 10 1,2,4-Tnchlorobenzene Nl3<500 25 <br /> Dibromomethane ND<500 1 0 5 0 1,1,1 Trichloroethane N1X500 5 0 <br /> 1,2-Dichlorobenzene ND<500 10 50 1,1,2-Trichloroethane ND<500 50 <br /> ' 1,3-Dichlorobenzene ND<500 10 5 0 Trichloroethene ND<500 1 0 5 0 <br /> 1,4-Dichlorobenzene ND<500 10 5 0 Trichlorofluoromethane ND<500 1 0 5 0 <br /> Dichlorodifluoromethane ND<500 1 0 5 0 1,2,3-Trichloropropane ND<500 10 50 <br /> l 1-Dichloroethane ND<500 1 0 5 0 1,2,4-Trimethylbenzene ND<500 10 5 0 <br /> ' 1,2-Dichloroethane ND<500 l0 50 1,3,5-Tnmethylbenzene ND<500 10 50- <br /> 1,1-Diehloroethene ND<500 t 0 5 0 Vinyl Acetate m ND<500 5 0 25 <br /> cis-1,2-Dichloroethene ND<500 1 0 50 Vinyl Chlonde ° ND<500 1 0 50 <br /> trans-l,2-DichloroethellL ND<500 1 0 50 Xylenes,total ND<500 1 0 5 0 <br /> 1,2-Dichloropropane ND<500 1 0 50 Comments <br /> 1,3-Dichloropropane ND<500 1 0 5 0 Surrogate Recoveries{%) <br /> 2,2-Dichloropropane ND<500 1 0 5 0 Dibromol]uoromethane 110 <br /> 1,l-Dichloropropene ND<500 1 0 5 0 Toluene-d8 105 <br /> ' cis-1,3-Dichloropropene ND<500 1 0 5 0 4-Bromotluorobenzene 98 <br /> water and vapor samples are reported in ugll soil and sludgi.samples in ug/kg,wipes in ug/wipe and all 1 CLP/SPLP extracts in ug/l <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-propananc or dimethyl ketone, (c) (2 chloroethoxy) etheic (d) 2-hexanone (e) dichloromethane (0 2-butanone, (g) d methyl <br /> pentanone of isopropylacetone (h)lighter than water immiscibic sheen is present (i)liquid Sample that contains greater than -5 vol <br /> sediment 0) sample diluted due to high organic Content (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes __ J <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> E <br />