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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 htLL/www mccampbell corn E-mail main@mccampbell corn Advanced GeoEnvlronmental Client Project ID Rain Water Carwash Date Sampled 04/30/01 i 837 Shaw Road Date Received 05/01/01 I ' Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 05102-05/04/01 Client P O Date Analyzed 05/02-05/04/0I ' BPA method$260 Volatile Organics By GC/MS Lab ID 66598 ' Client ID MW3/043001 Matrix W Reporting limit Repomng Limit Compound Concentration* W S Compound Concentration* I W S Acetone ih) ND<500 1 50 25 trans-l,3-Dechloropropene ND<500 10 50 Benzene ND<500 1 0 50 Ethylene dibromide ND<500 1 0 50 Bromobenzene ND<500 1 0 50 Bthylbenzene ND<500 1 0 50 ' Bromochlorometham. ND<500 1 0 50 Hexachlorobutadiene ND<500 50 25 Brorriodichloromethane ND<500 1 0 50 Iodomethane ND<500 1 0 50 Bromoform ND<500 1 0 50 Isopropylbenzene ND<500 1 0 50 Bromometbane ND<500 1 0 50 p-Isopropyl toluene N13<500 1 0 50 n-Butyl benzene ND<500 1 0 5 0Methyl butyl ketone ND<500 1 0 50 sec-Butyl benzene ND<500 10 50 tMethylene Chlonde` ND<500 1 0 50 Cert-Butyl benzene ND<500 l 0 50 Methyl ethyl ketone ND<500 20 10 Carbon Disulfide ND<500 l 0 50 Methyl isobutyl ketones ND<500 10 50 ' Carbon Tetrachlondi- - ND<500 l 0 50 Methyl tert-Butyl Fther(MTBF) ND<500 1 0 50 Chlorobenzene ND<500 l 0 5 0 Naphthalene ND<500 50 50 Chloroethane N13<500 l 0 50 n-Propyl benzene ND<500 l U 50 2-Chlorcethyl Vinyl hthW" ND<500 l 0 50 Styrenc ND<500 10 50 Chloroform — Nr)<500 l0 50 1,1,1,2-retrachloroethant. 14I 500 l0 50 Chloromethane ND<500 l0 50 1,1,2,2-Tetrachloroethane ND<500 10 50 2-Chlorotoluene NIK500 1-0 50 Tetrachloroethene ND<500 1 0 50 4 Chlorotoluene ND<500 1 0 50 Toluene ND<500 1 0 50 ' Dibromochloromethane N13<500 1 0 5(F 1,2 3-TnchlorobenzeneT ND<500 5 0 25 1,2-Dibromo-3-chlompropane ND<500 20 10 1,2,4-Tnchlorobenzene ND<500 1 5 0 25 Drbrorrioniethane ND<500 l0 50 1,1,1-Tnchloroethane ND<500 16 50 1,2-Dichlorobenzene N5<500 10 50 1,1,2-Tnehloroethane ND<500 10 50 1,3 Dichlorobenzene ND<500 l 0 50 Trichloroethene NI7<500 l 0 50 1,4-Dichlorobenzene ND<500 l 0 S D Tnchlorofluoromethane ND<500 ] 0 5 0 Dichlorodifluoromethane. ND<500 l0 50 1,2,3-Tnchloropropane ND<500 10 50 1 1-Dichloroethane ND<500 l 0 50 1,2,4-Tnniethylbenzene ND<500 10 50 ' 1,2-Dtehloroethane ND<500 l0 50 1,3,5-Trimethylbenzene ND<500 10 50 l,l-Dichloroethene ND<500 1 0 50 Vinyl Acetate m ND<500 5 0 25 cis-1,2-Dichloroethene ND1500 1 U —5O Viryl Chloride " 95<500 ] 0 5 0 trans-l,2-Dichloroethene ND<500 1 0 50 Xylenes,total ND<500 1 0 50 ' 12-Dichloropropane _ ND<500 1 0 50 Comments 1,3-Dichloropropane ND<500 1 0 50 Surrogate Recoveries(%) 22-Dichloropropane ND<500 1 0 50 Dlbromofluoromethane I,1-Dichloropropene ND<500 10 50 Toluene-d8 102 ' cis-1,3-Dichloropropene ND<500 10 50 4-Bromofluorobenzene _ 97 water and Vapor samples are reported in ug/1 soil and sludgt samples in ug/kg,wipes in ug/wipe and a]I FC I P/SPI P extracts in ug/l ND mo-ans nut(1V%,- led above the,icpui-ting limit N/A means analyte not applicable to this analysia (b) 2 proparium- ui dimethyl ketone (c) (2 41)loro,thmyJ ctherIL (d) 2 hexanone (c.) dichloromethanL, (t) 2-butanone (g) a-inethyi-? pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (1) liquid sample that contains greater than 5 vol sediment, 0) sample diluted due to high ornante eontent (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester (n) chloroethene (o)dimethylbenzenes DHS Certification No 1644 Edward Hamilton, Lab Director