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110 2nd Avenue South #D7 Pacheco - <br /> CA 94553 SS60 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' hM2//www mccamnbel!corn E-mail main@mccampbell com <br /> ' Advanced GeoEnvirotunental Client Project 1D Rain Water Car Wash Date Sampled 04/12/01 I_ <br /> 837 Shaw Road i Date Received 04/12/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 04/13-04/17/01 <br /> ' Client P O Date Analyzed 04/13-04/17/01 <br /> ' EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 65337 <br /> Client ID EW-I <br /> ' Matrix }fir <br /> # Rgniing Limet Reporting Limn <br /> Compound Concentration W S Compound Concentration* <br /> W 5 <br /> Acetone yet ND<1500 50 25 trans-1,3-Dichloropmpene ND<500 1 0 50 <br /> Benzene 1700 1 0 _-Y-0 Ethylene dibromide ND<500 1-0 5 0 <br /> Bromobenzene ND<500 to 5 0 Ethylbenzene 550 —T-0— 5 0 <br /> Bromochloromethane ND<500 10 5 0 Hexachlorobutadiene I ND<500 5 4 25 <br /> Brornodichioromethane ND<500 1 0 5 0 Iodomethane ND<500 1 0 50 <br /> Bromoform ND<500 1 0 5 0 lsopropylbenzene ND<500 1 0 50 <br /> Bromomethane ND<500 1 0 50 p-Isopropyl toluene ND<500 1 0 50 <br /> n-Butyl benzene ND<500 1 0 __5'_O Methyl butyl ketone ND<500 1 0 50 <br /> ' sec-Butyl benzene ND<500 1 0 5 0 Methylene Chlonde` ND<1500 1-0 5 0 <br /> tert-Butyl benzene ND<500 1 0 5 0 Methyl ethyl ketone ND<500 2 0 l0 <br /> N <br /> Carbon Disulfide 5<560 1 0 5 0 Methyl isobutyl ketone`x ND<500 1 0 5 0 <br /> Carbon Tetrachloride ND<500 1 0 5 0 Methyl tert-Butyl Ether(MTBE) — 1 0 5 0 <br /> Chlorobenzent. ND<500 1 0 5 0 Naphthalene _ ND<500 5 0 5 0 <br /> Chloroethane ND<500 1 0 5 0 n-Propyl benzene ND<500 10 5 0 <br /> 2 Lhlomethyl Vinyl E=ther ND<500 l 0 50 Styrene ai ND<500 1 0 5 0 1 <br /> Chloroform ND<500 l0 50 1,1,1,2-Tetrachloroethane ND<500 10 50 li <br /> ' Chloro _ 0methane _ ND<500 1 5 0 1,;,2 2-Tetrachloroethane ND<500 l 0 5 0 <br /> 2 Chlorotoluenc ND<500 1 0 5 0 Tetrachlorcethent, ND<500 1-0 5 0 <br /> 4-Chlorotoluene ND<500 ] 0 S 0 Toluene 4800 1-0 _yTJ <br /> Dibromochloromethane ND<500 _10 5 0 12 3-Tnehloroben7ene ND<500 5 0 25 <br /> 1 2-Dibromo-3-chlompropane ND<500 2 0 10 1.2,4-Tricltlorobenzene ND<S00 5 0 25 <br /> Dibromomethane ND<500 1 0 50 1,1 1-Trichloroethane ND<500 i 0 50 , <br /> 12-Dichlorobenzene ND<500 10 50 11,2-Tnchlomethane ND<500 l0 50 <br /> 1,3-Dichlorobenzene ND<500 10 50 Trichloroethene ND<500 10 50 <br /> ' 1,4-Dichlorobenzene ND<500 10 50 Trichlorofluoromethane 1 D7 10 50 <br /> Dichiorodtfluoromethane ND<500 1 0 __S7_0 1,2,3-Tnehloropropane ND<500 to 5 0 <br /> 1,1-Dchloroethane ND<500 10 50 1,2,4-Tnniethylbenzene ND<500 10 50 <br /> 1 2-Dichloruethane ND<500 1 0 5 0 1,3,5-Tnmethylbenzene LND<500 <br /> 1 0 5 0 <br /> ' l 1-Dichlaroethene N0<500 1 0 50 Vinyl Acetate _ 50 25 <br /> cis-1,2-D ehloroethene ND<500 00 —50 Vinyl Chlonde " 1 0 5 0 <br /> trans-1,2-Dtchloroethene ND<500 1 0 50 Xylenes,total 4 1 0 5.0 <br /> 12-Dichloropropane ND<500 1 0 5 0 Comments <br /> ' 1 3-Dichloropropane — ND<500 1 0 50 Surrogate Recoveries{%6) <br /> 2,2-Dichloropropane ND<500 1 0 5 0 Dibromofluct methane 96 <br /> 11-Dichioropropene N13<500 10 50 1 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<500 10 50 4-Brorrwfluorobenzene 98 <br /> ' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all I CLP/SPLP extracts in ug/l <br /> ND means not detected above the rLporting limit N/A means analyte not applicable to this analysis <br /> ' (b) 2-propanonL or dimethyl ketone, (c) (2�,hloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (t) 2-butanonL, (g) 4-tnethyl 2 <br /> pentanone or isopropylacetone (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol ',, <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl e%t[,r (ii) <br /> • chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 _Edward Hamilton, Lab Director <br /> i <br /> 3 <br />