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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ' McCA VIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hap//www mecampbell corn E-mail main@mccampbell com <br /> ' Advanced GeoEnvironmental Client Project ID Rainwater Car Wash I Date Sampled 12/21/00 <br /> ' 4005 North Wilson Way <br /> Date Received 12/27/00 <br /> Stockton, CA 95205 Client Contact Tlm Cuellar Date Extracted 12/29-01/03/01 <br /> Client P O Date Analyzed 12/29-01/03/01 <br /> Volatile Orgames By GC/MS <br /> EPA method 8260 <br /> ' Lab ID 56929 <br /> Client ID P10 108-1 it <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Repontrig Limit <br /> ' W S W S <br /> Acetone ND<2 5 50 25 trans-1,3-Dichloropropene ND<2 5 10 50 <br /> Benzene ND<2 5 to 5 0 Ethylene dibromide ND<2 5 to 50 <br /> ' Bromobenzene NIK2 5 to 50 Ethylbenzene - ND<2 5 l 0 50 <br /> Bromoebloromethane ND<2 5 10 1 50 Hexachlorobutadiene ND<2 5 5 0 25 <br /> Bromodichloromethane NIK2 5 to 50 iodomethane ND<2 5 1 0 5 0 <br /> Bromoform 3 4 10 50 Isopropylbenzene ND<2 5 1 0 5 0 <br /> Bromomethane ND<2 5 1 0 5 0 -p-Isopropyl toluene NIK2 5 10 5 0 <br /> ' n-Butyl benzene ND<2 5 10 5 0 Methyl butyl ketone ND<2 5 10 50 <br /> sec-Butyl benzene ND<2 5 10 5 0 Methylene Chloride"' ND<10 1 0 50 <br /> tent-Butyl benzene ND<2 5 10 5 0 Methyl ethyl ketone ND<2 5 2 0 10 <br /> '. Carbon Disulfide ND<2 5 10 5 0 Methyl isobutyl kctone k ND<2 5 1 0 5 0 <br /> Carbon Tetrachloride ND<2 5 10 5 0 Methyl tent-Butyl Ether(MTBL) 1 0 5 0 <br /> Chlowbenzenc ND-2 5 I 0 5 6 Naphthaiene ND<2 5 U 5 U <br /> Chloroethane ND<2 5 1 0 5 0 n-Propyl benzene ND<2 5 l 0 5 0 <br /> ' 2 Chloroethyl Vinyl 6t�hei" ND<2 5 - l 0 5 0 Styrene ND<2 5 l 0 5 0 <br /> Chloroform ND<2 5 10 50 1,1,1,2-Tetrachloroethane ND<2 5 l 0 50 <br /> _Chloromethane ND<2 5 l 0 5 0 1 1,2,2-Tetrachloroethane ND<2 5 l 0 50 <br /> i 2-Chlorotolluene _ NIK2 5 10 50 Tetrachloroethene _ 97 1-0 5 0 <br /> ' 4-Chlorotoluene - ND<2 5 10 50 Toluenc ND<2 5 1 0 5 0 <br /> Dibromochloromethane ND<2 5 1-0 5 0 1,2,3-Tnchlorobenzene ND<2 5 510 25 <br /> 1,2-Dibromo-3-chloropropane ND<2 5 20 10 1,2,4-Tnchlorobenzene ND<2 5 25 <br /> Dtbromomethane ND<2 5 10 50 1,1,1-Tnchloroethwe ND<2 5 50 <br /> ' 1,2-Dtchlorobenzene - ND<2 5 10 5 0 1,1,2-Tnchloroethane ND<2 5 5 0 <br /> I <br /> 1,3-Dichlorobenzene ND<2 5 10 5 0 Trichloroethene ND<2 5 50_ <br /> 1,4-Dichlorobenzene ND<2 5 10 5 0 Trichlorofluoromethane. ND<2 5 5 0 <br /> DichlorodilluoromethanL ND<2 5 10 5 0 1,2,3-Trichloropropane N1X2 5 1 0 5 0 <br /> 1,1-Dichloroethane -- ND<2 5 10 5 0 1,2,4-Tnmethylbenzene i ND-2 5 1 0 5 0 <br /> I Droethane N71 2 5 10 50 1,3,5-Tnmethylbenzene ND<2 5 ___10 5-0-1 <br /> 1 l-Dichloroethene ND<2 5 10P50 <br /> Vinyl Acetate °' NDt2 5 5 0 25 <br /> ws-1 2-Dichloroethene ND<2 5 10 Vinyl Chloride " ND<2 5 1 0 50 <br /> trans-1,2-Dichloroethene ^� ND<2 5 10 Xylenes,total ND<2 5 1 0 5 0 <br /> 1,2-Dichloropropane ND<2 5 10 Comments <br /> 1 3-Dichloropropane ND<2 5 iD Surrogate Recoveries2,2-Dichloropropane ND<2 5 10 Dibroniofluoromethane 106 <br /> ' 1,1-Dichloropropene ND<2 5 10 50 TolueneA8 - — _ 99 <br /> cis-1,3-Dichloropropene ND<2 5 1 0 5 0 4 Bromofluorobenzene 103 <br /> water and vapor samples are reported in ug/L soil and sludge samples in ug(kg,wipes in ug/wipe and d11 1( [P!SPLP LxtraLts in ugrt <br /> ' NI7 means not detected above 1hL reporting limit N/A means analyte not apphcabic to this analysis <br /> (b) 2-propanonL or dimethyl ketone (L)(2-chloroethoxy)ethenc (d) 2-hexanone ((,)dithloromLthane (t) 2-butanone (g) 4 methyl 2 <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than -5 Nol °'" <br /> sediment, (1) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> ' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />