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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 ' 24 http//www mccampbell corn E-mail main@mccampbcll com ' Advanced GeoEnvironmental Client Project ID Rainwater Car Wash IDate Sampled 12/18/00 i 4005 North Wilson Way Date Received 12/20/00 ' Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 12/21-12122/00 i Client P O Date Analyzed 12/21-12/22/00 Volatile Organics By GC/MS � 1 EPA method 8260 T Lab ID 56431 _ ' Client ID P7 129-132 Matrix W Reporting Limit Reporting Limit Compound Cancentrabon'i W S Compound Concentration* Reporting S ' Acetone ibt ND 50 25 trans-l,3-Diebioropropene ND<5 0 10 50 Benzene ND<5 0 1 0 50 Ethylene dibromide ND<5 0 10 50 Bromobenzene ND<5 0 1 0 50 Ethylbenzene ND<5 0 10 50 ' Bromochloromethane ND<5 0 1 0 50 Hexachlorobutadiene ND<25 50 25 Bromodichloromethane ND<5 0 1 0 50 1 lodomethsne ND<5 0 10 50 Bromoform ND<S 0 1 0 50 lsopropylbenzene ND<5 0 10 50 Bromomethane ND<5 0 1 0 50 p-Isopropyl toluene ND<5 0 10 50 ' n-Butyl benzene ND<5 0 1 0 5 0 Methyl butyl ketone --- ND<5 0 IQ 50 sec-Butyl benzene ND<5 0 l 0 50 Methylene Chloride(') ND<25 to 50 Cert-Butyl benzene ND<5 0 1 0 50 Methyl ethyl ketone ND<10 20 10 Carbon Disulfide ND<5 0 l 0 5 0 Methyl isobutyl ketone 8 ND<5 0 10 5 0 Carbon Tetrachloride ND<5 0 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 5 0 Chlorobenzene ND<5 Q 1 U 50 Naphthalene ND<l5 �5 U ti U Chloroethane ND<5 0 1 0 5 0 n-Propyl benzene ND<5 0 1 0 5 U 2-Chloroethyl Vinyl RbLt" ND<5 0 1 0 50 Styrene ND<5 0 1 0 5 0 ' Chloroform _ ND<5 0 ] 0 5 0 1,1,1 2-Tetrachloroethane ND<5 010 5 0 Chloromethane ND<5 0 1 0 5 0 1,1,2,2-Tetrachloroethane NDc5 0 1 0 5 0 2-Chlorotoluene ND<S 0 1 0 5 0 Tetrachloroethene 330 10 5 0 4-Chlorotoluene ND<5 0 1 0 50 Toluene ND<5 0 10 5 0 t Dtbromochloromethane ND<5 0 1 0 5 0 1,2,3-Trichlorobenzene� ND<25 50 25 1,2-Dibromo-3-chloropropane NDK10 2 0 10 1,2,4-Tnehlorobenzenc NLK25 50 25 Dibromomethane ND<5 0 1 0 50 1 l,]-Tnchloroethane T ND<5 0 10 50 ' 1,2-Dichlorobenzene - ND<5 11 10 50 1 1,1,2-Tnchloroethane _— ND<511 10 50 1,3-Dichlorobenzene ND<5 0 r10 50 Trichloroethene ND<5 0 10 50 1,4-Dichlorobenzene ND<5 0 50 Tncltlomfluoromethane ND<5 0 1 0 so Dichlorodifluoromethane ND<5 0 5 0 1,2,3-Tnchloropropane ND<5 0 10 5 0 1,1-Dtchloroethane ND<5 6 10 1,2,4-TrND<5 0 10 50 ' 1,2-Dichloroethane ND<5 0 5 0 1,3,5-Tnmethylbenzene ND<5 0 10 50 1 1-Dichloroethene ND<5 0 5 0 Vinyl Acetate n ND<25 50 25 cis-1,2-Dtchloroethene ND<5 0 1 0 50 Vinyl Chloride i°' ND<5 0 10 50 ' trans-1 2-Dtchlomethene - ND<5 0 1 0 50 Xylenes,total ND<5 0 ] 0 S D I,2-Dichloropropane ND<5 0 1 0 5 0 Comments 1,3-Dichloropropane ND�5 0 1 0 50 Surrogate Recoveries(%) 2,2-Dichioropropane ND<5 0 1 0 5 0 Dibromofluoromethane l Ofi ' 1,1-Dichloropropene ND<5 0 1 0 50 Toluene-d8 —- - lot 1 LIS-] 3 Dichloropropene NIKS Q 1 0 5 0 4-Bromofluorobenzene 102 water and vapor samples art,reported in ug/1 soil and Sludge samples in ug/kg,wipes in ug/wipe and all TL l P/SPLI't.xtraLts in ug/i ND means not detected above the reporting limit NIA means analyte not applicable to this analysis (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) d:chloromethane (1) 2 butanone (g) 4-methyl 2 pentanonc or isopropy]acetone (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than -5 vol °4 II sediment (J} sample diluted due to high organic Lontent (k) ethenylbenzene (l) methylbenzene, (in) acetic acid ethenyl tstcr (n) chloroethene (o)dimethylbenzenes ' DHS Certification No 1644 _Edward Hamilton, Lab Director 1