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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-I620 Fax 925-798-1622 <br /> ' http//wwwmccyinpbellcom E-mail mam@mccampbell com <br /> Advanced Geo)tinvuonmenta3 Cheat Project LD Rainwater Car Wash <br /> Date Sampled 12/20/00 <br /> 4005 North Wilson Way Date Received 12/22/00 <br /> Stockton, CA 95205 Client Contact Tun Cuellar i Date Extracted 12/23-12/26/00 <br /> Client P O Date Analyzed 12/23-12/26100 <br /> EPA method 8260 Volatile Organics By GC/MS <br /> ' Lab ID 56688 <br /> Client ID P94447 <br /> Ma pr <br /> Compound Concentration* Reporting L'St Compound Concentration* Reponsng Limit <br /> _ W 5 <br /> Acetone } ND<30 50 25 trans-1,3-Dichkoropropene ND<10 1 0 5 0 <br /> Benzene ND<10 1 0 5 0 Ethylene dibromide ND<10 l 0 5 0 <br /> 13romobenzene ND<l0 1 0 50 Ethylbenzene ND<10 ] 0 50 <br /> I ' Bromochloromethane ND<10 1 0 5 0 Hoxachlombutadiene _NIX 10 50 25 <br /> Bromodtchioromethane ND<10 —10 5 0 iodamethane ND<10 i 0 50 <br /> Bromoform ND<10 1 0 5 0 lsopropylbenzene ND<l0 1 0 50 <br /> Bromomethane ND<10 1 0 50 p-Isopropyl toluene ND<10 1 0 5 0 <br /> ' n-Butyl benzene ND<10 t 0 5 0 Methyl butyl ketone' ND<10 1 0 56-- <br /> see-Butyl <br /> 0sec-Butyl benzene ND<10 1 0 50 Methylene Chloride` NIK30 ] 0 50 <br /> tert-Butyl benzene ND<10 1 0 50 Methyl ethyl ketone ND<10 2 D 10 <br /> Carbon Disulfide ND<10 1 0 50 Methyl isobutyl ketone'K ND<10 1 0 —50 <br /> lie Carbon Tetrachlondr ND<10 1 0 50 Methyi tent-Butyl Ether(MTBE) -- 10 5 0 <br /> Chlorobenzene NTX10 1 0 50 Naphthalene <I0<I _J10 5 0 <br /> Chloroethane ND<10 ] 0 5 0 -n-Propyl benzene ND<10 l 0 50 <br /> 2Lhlomethyl Vmyl Ether` ND<10 1-0 5 0 Styrene MND<10 1 0 5 0 <br /> ' Chloroform ND<10 1 0 50 1,1,42-Tetrachloroethane ND7<10 t 0 50 <br /> Chloromethane ND<10 1 0 50 1,1,2,2-Tetrachloroethane ND<10 1-0 —50 <br /> 2 Chlorotoluene ND<10 1 0 50 Tetrachloroethene 220 1 0 5 0 <br /> 4-Chlorotoluene NEXIO 1 0 5 0 Toluene ND<]0 _10 5 0 <br /> Dibromochloromethane ND<10 1 0 50 1,2,3-Tnchlorobetizene N[<lo 50 25 <br /> 1,2 Dibromo-3-chloroprapane NDc10 2 0 10 1,2,4-Trichlorobenzene ND<10 5 0 25 <br /> Dibromomethane ND<10 10 50 1,1,1-Tnehlowethane _ ND<10 _10 5 0 <br /> en <br /> ' 1,2-Dichlorobzene ND<10 l0 50 1,1,2-Tnchloroethane ND<10 10 50 <br /> 1,3-Dichlorobenzene ND<10 10 5 0 Trichloroethene ND<10 1 0 5 0 <br /> 1 4-Dichlorobenzene ND<10 10 __5__O Tnchlorofluoromethane _ ND<lfl _10 5 0 <br /> Dichlorodifluorornethane ND<10 10 50 1,2,3-Tncblompropane ND<10 ] 0 S Q <br /> ' l l-Dichloroethane ND<10 1 0 5 D 1,2,4-Trrmethylbenzene N <br /> — D<l0 1-0 S D <br /> 12 Dichloroethane ND<10 1 0 50 1,3,5-Trimethylbenzene ND<10 1-0 5 0 <br /> ],I-Dichloroethene ND<16 1 0 5 0 Vinyl Acetate m ND<10 to <br /> 25 <br /> cis-1,2-Drchloroethene ND<10 10 5 0 Vinyl Chloride " ND<10 50 <br /> trans-l,2-Dichloroethene ND<10 10 50 Xylenes,total Nb<10 —5 0 <br /> 1,2 Drchloropropane ND<10 1 0 5 0 Comments <br /> 1,3-Drchloropropane _ NIK 10 1 0 5 0 Surrogate Recoveries(%) <br /> 2 2 Dichlaropropane ND<10 to 5 0 Drbromafluoromethane 105 <br /> ' 1,1 Dichloropropene ND<10 l 0 50 Toluene d8 100 _� <br /> cis-k,3-Dichloropropene NIK10 10 50 4-Bromofluorobenzene 102 <br /> water and vapor samples are reported in ug/1 soil and sludge samples in ug/kg,wipes in ug/wipc and all TC'LP/SPLP extracts in ugri <br /> ' ND mems riot detected above the reporting limit N/A means analyte not applicable to this analysis i <br /> (b)2-propanone or dimethyl ketone (c,) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane. (f)2-butanotic (g) 4-methyl '_ <br /> pi ntarione or isopropylacetone (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than –5 vol <br /> sediment V) sample diluted due to high organic content (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes m- f <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />