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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ' MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Mtn be3l//www.mccampcom E-mail main@mccampbelI com <br /> Advanced GeoEnvironinental Client Project ID Rain Water Car Wash hate Sampled 01130/02 <br /> ' 837 Shaw Road Date Received 01/31/02 <br /> Stockton, CA 95215 CIient Contact Tim Cuellar Date Extracted 0 1/3 1/02 <br /> Client P O Date Analyzed 02/05/02 <br /> Lead* <br /> LE—PAanalytiew methods 6010200 7,239.2* <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 89351 GAC 2 W TTLC ND N/A <br /> ' 89352 Influent W TTLC ND N/A <br /> 89353 Effluent W TTLC ND N/A <br /> Reporting Limit unless S rTLC g 3 0 mg/kg -� <br /> otherwise stated ND means not — — <br /> detected above the reporting W TTLC -i 0 005 mg/L '� <br /> ' limit STLC,TCLP <br /> 0.2 mg1L <br /> •soil and sludge samples are reported in mg/kg,wipe samples m ug/wipe and water samples and all STLC I SPLP I TCLP extracts in mgll <br /> ' 'Lead is analysed using EPA method 6010 (ICP)fm soils sludges, STLC & TCLP extracts and method 2392 (AA Furnace) for water <br /> samples <br /> a DISTLC extractions are performed using STLC methodaiogy except that deionurd water is substituted for citnc acid buffer as thL <br /> extraction fluid DISTLC results are not applicable to STI_C regulatory limits <br /> i <br /> EPA extraction methods 131 1(TCLP) 3010/3020(water TTi Q 3040(organic matrices T n-C) 3050(solids M,C) Sl LC LA f itle 72 <br /> "surrogate diluted out of range N/A means surrogate not applicable to this analysis <br /> • i " repornng limit raised due to matrix interference <br /> I) liquid sample that contains greater than -2 vol % sediment this sediment is extracted with the liquid in accordance with I P 1 <br /> L meth odolo ies and can simificantly effect reported metal concentrations <br /> DHS Certification No 1644 —I&L7Edward Hamilton, Lab Director <br />