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BSKANALYTICAL <br /> LABORATORIES <br /> Jim Phillips Certificate of Analysis <br /> Castle Analytical Laboratory ELAP Certificate#1180 <br /> 2333 Shuttle Dnve Report issue Date 03/12/2003 <br /> Atwater, CA 95301 <br /> BSK Submission#: 2003021643 <br /> ' BSK Sample ID #: 297385 <br /> Project II) 5494 Project Desc Rainwater Car Wash <br /> Submission Comments <br /> Sample Type Liquid Date Sampled 02/24/2003 <br /> Sample Description Effluent Time Sampled <br /> Sample Comments Date Received 02/28/2003 <br /> ' Inorganics prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> ' Lead(Pb) EPA6010A ND mg/L 005 1 005 03/10/03 03/11/03 <br /> I <br /> ' mg/L Milligrams/Liter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result <br /> ' lig/L Micrograms/Liter(ppb) PQL x Dilution S Suspect result See Cover Letter for comments <br /> pg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysis performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> ' <br /> Report Authenncation Code IIIIIIII1111VIIOU 111IQmBII Milo IN 11111111111111 Page 1 of 1 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935 <br />