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1 <br /> ' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384--1507 <br /> Advanced GeoEnvironmental Inc Client Project ID Rainwater Car Wash Sampled 11-11-02 <br /> of Northern California Reference Number 5218 Received 11-12-02 <br /> 837 Shaw Road Sample Description Water Extracted 11-14-02 <br /> ' Stockton,CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 11-14-02 <br /> ARn Tim Cuellar Lab Number 5218-3W Reported 11-26-02 <br /> Client Sample ID MW 3111-11-02 <br /> VOLATILE ORGANICS -EPA METHOD 8260 GCIMS <br /> REPORTING SAMPLE REPORTING SAMPLE <br /> ' ANALYTE LIMIT" RESULT ANALYTE LIMIT" RESULT <br /> ( /L) <br /> Benzene 050 ND 1,3-Dichloro ro ane 050 ND <br /> Bromobenzene 050 ND 2,2-Dichloro ro ane 050 ND <br /> ' Bromochloromethane 050 ND 1,1-Dichloro ro ene 050 NO <br /> Bromodichloromethane 050 NO cis-1 3-Dichloro ro ene 050 NO <br /> Bromofomi 050 ND trans-1,3-Dichloro roene 050 ND <br /> Bromomethane 050 NO Eth lbenzene 050 ND <br /> ' n-But (benzene 050 ND Hexachlorobutadiene 050 ND <br /> —sec-Butylbenzene 050 ND lsopropylbenzene 050 ND <br /> tert-But lbenzene 050 ND p-Isopropyltoluene 050 ND <br /> Carbon tetrachloride 050 ND Methylene chloride 250 ND <br /> ' Chlorobenzene 050 NO Methyl tent-Butyl Ether MTBE 050 630 <br /> Chlorodibromomethane 050 ND Na thalene 1 00 NO <br /> Chloroethane 050 ND n-Propylbenzene 050 ND <br /> Chloroform 050 ND -Styrene___ 0 50 ND <br /> Chloromethane 050 ND 1,11 2-Tetrachloroethane 050 ND <br /> 2-Chlorotoluene 050 NO 1 1 2 2-Tetrachlorethane 050 ND <br /> 4-Chlorotoluene 050 ND Tetrachloroethene PCE 050 24, <br /> 1 2-Dibromo-3-chloro ro ane 050 NO Toluene 050 NO <br /> ' 1 2-Dibromoethane(EDB) 050 NO 1,2 3-Trichlorobenzene 050 ND <br /> Dibromomethane 050 ND 1,2,4-Trichlorobenzene 050 ND <br /> 1,2-Dichlorobenzene 050 ND 1,1,1-Trichloroethane 050 NO <br /> 1 3-Dichlorobenzene 050 NO 1 1 2-Trichloroethane 050 ND <br /> ' 1,4-Dichlorobenzene 050 ND Trichloroethene CrCE 050 090 <br /> Dichlorodifluoromethane 050 ND Trichlorofluoromethane 050 NO <br /> 1 1-Dichloroethane 050 ND 1 2 3-Trichloro ro ane 050 NO <br /> 1 2-Dichloroethane 050 ND 1,2,4-Trimeth lbenzene 050 NO <br /> ' 1 1-Dichloroethene 050 ND 1,3,5-Trimeth lbenzene 050 NO <br /> cis-1,2-Dichloroethene 050 ND Vinyl Chloride 050 NO <br /> trans-1 2-Dichloroethene 050 ND Xylenes.total 050 NO <br /> 1 2-Dichloro ropane 050 ND <br /> ' "Deport Limit Multiplication Factor 1 <br /> "Report Limit Multiplication Factor for MTBE 20 <br /> Surrogate Recoveries <br /> ' Dibromofluoromethane 127% Toluene-d8 102% <br /> 1 2-Dichloroethane-d4 112% p-Bromofluorobenzene 925% <br /> Instrument ID HP 5972 MS <br /> ' Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (fig/L)= micrograms per liter or parts per billion(ppb) <br /> ANALYSTL&df- r� APPROVE=D BY <br /> Clary J ne mss C Phillips <br /> Laboratory Director <br />