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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> ' Advanced GeoEnvironmental Inc Chent Project ID Rainwater Car Wash Sampled 11-10-02 <br /> of Northern California Reference Number 5218 Received 11-12-02 <br /> 837 Shaw Road Sample Description Water Extracted 11-14-02 <br /> ' Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 11-14-02 <br /> Attn Tim Cuellar Lab Number 5218-8W Reported 11-26-02 <br /> Client Sample lD MW 9B/11-10-02 <br /> ' VOLATILE ORGANICS-EPA METHOD 8260 GC1MS <br /> REPORTING SAMPLE REPORTING SAMPLE <br /> ANALYTE LIMIT' RESULT ANALYTE LIMIT* RESULT <br /> IL ( /L /L /L <br /> Benzene 050 ND 1,3-Dichlororoane 050 ND <br /> Bromobenzene 050 ND 2 2-Dtchlororo ane 050 ND <br /> ' Bromochloromethane 050 ND 1,1-Dichloro ro ene 050 ND <br /> Bromodichloromethane 050 ND cis-1,3-Dtchloro ro ene 050 ND <br /> Bromoform 050 ND trans-1 3-Dtchloro ra ene 050 ND <br /> Bromomethane 050 ND Eth (benzene 050 ND <br /> ' n-But (benzene 050 ND Hexachlorobutadtene 050 NO <br /> sec-But lbenzene 050 ND Isopropylbenzene 050 ND <br /> tert-Bu lbenzene 050 ND p-Isopropyltoluene 0 50 ND <br /> Carbon tetrachloride 050 ND Methylene chlonde 250 ND <br /> ' Chlorobenzene 050 ND Methyl tert-Butyl Ether MTBE 050 16 <br /> Chlorodibromomethane 050 ND Na thalene 1 00 ND <br /> Chloroethane 050 ND n-Propylberizene 050 ND <br /> Chloroform 050 3 9 Styrene 050 ND <br /> Chloromethane 050 ND 1,1,1,2-Tetrachloroethane 050 ND <br /> 2-Chlorotoluene 050 ND 1,1 2,2,-Tetrachicrethane 050 ND <br /> 4-Chlorotoluene 050 ND Tetrachloroethene PCE 050 170 <br /> 1,2-Dibromo-3-chloro ro ane 050 ND Toluene 050 1 2 <br /> ' 1 2-Dibromoethane(EDB) 050 ND 1,2 3-Tnchlorobenzene 050 ND <br /> Dibromomethane 050 ND 1,2,4-Trichlorobenzene 050 ND <br /> 1 2-Dichlorobenzene 050 ND 1 1 1-Trichloroethane 050 ND <br /> 1 3-Dichlorobenzene 050 ND 1,1,2-Trichloroethane 050 ND <br /> ' 1 4-Dichlorobenzene 050 ND Trichloroethene CE 050 21 <br /> Dichlorodifluoromethane 050 NO Trichlorofluoromethane 050 NO <br /> 1 1-Dichloroethane 050 NO 1,2,3-Tnchloro ro ane 050 N❑ <br /> 1 2-Dichloroethane 050 ND 1,2,4-Trimeth lbenzene 050 ND <br /> ' 1,1-Dichloroethene 050 NO 13,5-Trimeth lbenzene 050 NO <br /> cis-1 2-Dichloroethene 050 1 2 Vin I Chloride 050 ND <br /> trans-1,2-Dichloroethene 050 NO Xylenes,total 050 ND <br /> 1,2-Dichloro ro ane 050 ND <br /> ' *Report Limit Multiplication Factor 1 <br /> *Report Limit Multiplication Factor for PCE 5 <br /> Surrogate Recoveries <br /> Dibromofluoromethane 123% Toluene-d8 1010% <br /> 1,2-Dichloroethane-d4 972% p-Bromofluorobenzene 875% <br /> Instrument ID HP 5972 MS <br /> ' Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> • (pg1L)= micrograms per liter or parts per billion(ppb) <br /> ' ANALYST APPROVED BY <br /> Clan J Cone J C Phillips <br /> aborafory Director <br /> I� <br />