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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> Advanced GeoEnvironmental, Inc Client Protect ID Rainwater Car Wash Method EPA 5030/8015M 8020 <br /> ' of Northern California Reference Number 5165 Instrument ID Var-GC1 <br /> 837 Shaw Road Sample Description Water Extracted 10-25-02 <br /> Stockton CA 95215 Analyst Jim Phillips Analyzed 10-25-02 <br /> Attn Tim Cuellar Reported 10-31-02 <br /> r <br /> ' QUALITY CONTROL DATA REPORT <br /> ' ANALYTE Gasoline MTBE Benzene Toluene Ethyl Benzene Total Xylenes <br /> Spike Concentration 110 210 1 32 7 94 1 84 922 <br /> Units ug/L ug/L ug/L ug/L ug/L ug/L <br /> LCS Batch# VW-0252 VW-0252 VW-0252 VW-0252 VW-0252 VW-0252 <br /> LCS %Recovery 118% 916% 910% 917% 101% 958% <br /> Surrogate Recovery 978% 964% 964% 964% 964% 964% <br /> Control Limits 70-130% 70-130% 70-130% 70-130% 70-130% 70-130% <br /> MSIMSD Batch# VW-0252 VW-0252 VW-0252 VW-0252 VW-0252 VW-0252 <br /> Spike Concentration 110 210 1 32 794 1 84 922 <br /> ' MS%Recovery 106% 104% 102% 914% 101% 962% <br /> Surrogate Recovery 102% 991% 991% 991% 991% 991% <br /> MSD%Recovery 108% 101% 101% 910% 100% 963% <br /> ' Surrogate Recovery 978% 954% 954% 954% 954% 954% <br /> Relative% Difference 154% 290% 0789% 0349% 0923% 0064% <br /> ' Methanol Blank ND ND ND ND ND ND <br /> Surrogate Recovery 951% 970% 970% 970% 970% 970% <br /> The LCS(Laboratory Check Sample)is a control sample of known, interferent free matrix that is fortified with representative analytes and <br /> ' analyzed using the same reagents,preparation and analytical methods employed for the samples The LCS%recovery is used for validation <br /> of sample batch results Due to matrix effects,the OC limits and recoveries for MSIMSD's are advisory only and are not used to acceptor <br /> or <br /> reject batch results <br /> ANALYST APPROVED BY <br /> Clan J Gone am0 C,P rIlrps <br /> L oratory Director <br /> I <br />