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' 110 2nd Avenue South YD7,Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798 1620 Fax 925-798-1622 <br /> http://www trccampbell corn E mail mom bel]com <br /> Advanced GeoEnvlronmental,Inc Client Project ID Rainwater CarWash Date Sampled 12/12/02 <br /> 837 Shaw Road Date Received 12/13/02 <br /> ' Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 12/19102-12120/02 <br /> Client P O Date Analyzed 12119/02-12/20/02 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Osler 0212252 <br /> Lab ID 0212252-002B <br /> ' Client ID GAC-2 <br /> Matrix Water <br /> Compound Concentration* DF Comraound Concentration* DF RporilLunn s <br /> ' Acetone ND 10 50 1 tert-Am l methyl ether AME ND 10 05 <br /> Benzene ND 10 0 5 Bromobenzene ND 10 05 <br /> i <br /> Bromochloromethane ND 10 05 Bromodichloromethane ND 10 0 5 <br /> Bromofonn ND 1 0 05 Bromomethane ND to 05 <br /> ' 2-Butanone MEK ND 1 0 1 0 t-Bu 1 alcohol(TBA) ND 10 5 0 <br /> n-Bu ]benzene ND 1 0 05 sec-Butyl benzene ND 10 0 5 <br /> tert-Butyl benzene ND 1 0 05 Carbon Dtsulfide ND 10 05 <br /> ' Carbon Tetrachlonde ND 1 0 05 Chlorobenzene ND 10 0 5 <br /> Chloroethane ND 1 0 05 2-Chloroeth l Vinyl Ether ND 10 0 5 <br /> Chloroform ND 1 0 0 5 Chloromethane ND 10 0 5 <br /> 2-Chlorotoluene ND 1 0 0 5 4-Chlorotoluene ND 10 0 5 <br /> Dibromochloromethane ND 1 0 05 1,2-Dibromo-3-chloro roane ND 10 05 <br /> 1,2-Dibromoethane EDB) ND 1 0 0 5 Dibromomethane ND 10 05 <br /> 1,2-Dichlorobenzene ND 1 0 05 1,3-Dichlorobenzene ND 10 0 5 <br /> 1,4-Dichlorobenzene ND 1 0 05 Dichlorodifluoromethane ND 10 05 <br /> ' 1,1-Dichloroethane ND 1 0 05 1,2-Dichloroethane 1,2-DCA ND to 05 <br /> 1,1-Dichloroethene ND 1 0 05 cls-1,2-Dichloroethene ND to 0 5 <br /> trans-l,2-Dichloroethene ND 1 0 05 1,2-Dichloro ro ane ND 10 05 <br /> 1,3-Dichloro ro ane ND 1 0 05 2,2-Dichlororoane ND 10 05 <br /> ' l,i-Dichloro ro ene ND 1 0 0 5 cis-l,3-Dichloro roene ND 10 0 5 <br /> trans-l,3-Dichloro ro ene ND 1 0 0 5 Dilso ro 1 ether(DIPS) ND 10 0 5 <br /> Eth lbenzene ND 1 0 05 Ethyl tert-but l ether ETBE ND 10 o5 <br /> Hexachlorobutadiene ND 1 0 05 2-Hexanone ND 10 05 <br /> ' Iodomethane Methyl iodide ND 1 0 0 5 lolmropyrlbenzene ND 10 0 5 <br /> 4-Isopropyl toluene ND 1 0 05 Meth l-t-bu l ether TBE ND 10 05 <br /> Methylene chloride ND 1 0 0 5 4-Meth 1-2- entanone M03K) ND 10 05 <br /> Na hthalene ND 10 0 5 n-Pro yl benzene ND to 05 <br /> ' <br /> Styrene ND 10 05 1,1,1,2-Tetrachloroethane ND 10 0 5 <br /> 1,1,2,2-Tetrachloroethane ND to 05 Tetrachlomethene ND 10 0 5 <br /> Toluene ND 10 05 1,2,3-Tnchlorobenzene ND 10 0 5 <br /> 1,2,4-Trichlorobenzene ND 10 0 5 1,1,1-Trichloroethane ND 10 05 <br /> 1,1,2-Trichloroethane ND 1 0 0 5 Trichloroethene ND 10 0 5 <br /> Trichlorofluoromethane ND 1 0 0 5 1,2,3-Trichlororoane ND 10 0 5 <br /> 1,2,4-Tnmeth lbenzene ND 1 0 0 5 1,3,5-Tnmeth lbenzene ND 10 0 5 <br /> Vinyl Acetate ND 10 50 1 Vinyl Chloride NO 10 0 5 <br /> ' Xylenes— ND J 1 0 05 <br /> Surrogate Recoveries(%) <br /> %SS 1 1 I 1 %SS2 103 <br /> ' %SS3 927 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in VgIL,soil/sludge/solid samples in ug/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> ' organic content <br /> ' DHS Certification No 1644 Edward Hamilton,Lab Director <br />