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110 2nd Avenue South 1lp7 Pacheco CA 44553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798 1622 <br /> ' hnp 1lwww mccampbell cam E mad main a nccampbcll coin <br /> QC SUMMARY REPORT FOR SW8260B <br /> Matrix W WorkOrder 0212252 <br /> ' EPA Method SW8260B Extraction SW5030B BatchlD 5317 Spiked Sample ID NIA <br /> Sample <br /> Compound Spiked MS'" MSD' MS-MSD' LCS Lr-SD ILCS-LCSD Acceptance Criteria(%) <br /> ' <br /> uglL pg/L %Ree %Rec %RK) % Ret % Ren %RPD Low High <br /> Benzene N/A 10 NIA NIA NIA 118 109 I 782 70 130 <br /> ' tert-Amyl methyl ether(TAME) NIA I 10 N/A ! N/A _ N/A 921 79 1 i 152 70 130 <br /> Chlorobenzene N/A 10 NIA NIA N/A 114 107 638 1 70 130 <br /> I,1-Dichloroethene N/A 10 NIA NIA NIA 872 805 803 i 70 130 <br /> Methyl-t-butyl ether(MTBE) N/A 10 N/A NIA N/A i 104 954 879 70 130 <br /> Toluene N/A 10 NIA NIA NIA 113 104 8 19 70 I 130 <br /> ' Trichloroethene N/A 10 NIA j NIA NIA 89 813 903 I 70 130 <br /> Dnsopropyl ether(DIPE) N/A 10 N/A NIA NIA 113 104 7 93—_..7 70 i 130 <br /> Ethyl tert-butyl ether(ETBE) N/A 3 10 N/A� N/A -N/A i 93 _ 863 1 744 70 i 130 <br /> %SSI N/A 100 NIA NIA NIA 966 946 I 213 _ 70 I 130 <br /> ' . %SS2 N/A 100 NIA N/A - N/A 105 105 0108 70 i 130 <br /> %SS3 N/A 100 NIA NIA NIA. I 109 110 1 03 70 130 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions <br /> NONE <br /> 1 <br /> 1 <br /> 1 <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPO=Relative Percent <br /> ' Deviation <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matnx or sample diluted due to high matrix or <br /> ' analyte content <br /> %Recovery=100`(MS Sample)/(Amount Spiked),RPD=104.(MS-MSD)I(MS+MSD)'2 <br /> 'MS and 1 or MSD spike recoveries may not be near 100%or the RPDs near 0°/n if a)the sample is inhomogenous AND contains significant concentrations of <br /> ' analyte relative to the amount spiked orb)d that specific sample matrix interferes with spike recovery I <br /> i <br />