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t110 2nd Avenue South,#1)7,Pacheco CA 94553 5560 <br /> I A# McCampbell Analytical Inc Telephone 925 798-1620 Fax 925-798-1622 <br /> http//www mccampbelt corn E-mail main@mccampbell corn <br /> ' Castle Analytical Laboratory Chent Project ID #4951, Rainwater Car Date Sampled 08/05/02 <br /> Wash <br /> 2333 Shuttle Drive Bldg 908/909 Date Received 08/08/02 <br /> ' Atwater,CA 95301 Client Contact James Phillips Date Extracted 08/08/02 <br /> Client P O Date Analyzed 08/08/02 <br /> ' Lead by Graphite Furnace Atomic Absorption* <br /> tiacnon method E200 9 Analytical methods E200 9 Work Order 0208113 <br /> ' Lab ID Client ID Matrix Extraction Lead DF %SS <br /> 0208113-OOIA Effluent W TTLC ND 1 N/A <br /> � II <br /> Reporting Limit for DP'=1, W TTLC 0 005 Mg/L <br /> ' ND means not detected at or <br /> above the reporting limit S TTLC NA mg/kg <br /> *water samples are reported in mg/L,soil/sludge/solid/product samples in in 91 wipes in uglmpe and all TCLP 1 STLC/DISTLC/SPLP extracts in <br /> mg/L <br /> ' ND means not detected above the reporting limit,NIA means not applicable to this sample or instrument <br /> Analytical Methods EPA 60tOC/200 7 for all elements except 200 9(water-Sb,As,Pb,Se,TI),245 1 (Hg),7010(sludge/soil/solid/oillproduct/wipes- <br /> ' As,Se,TI),747IB(Hg) <br /> DISTLC extractions are performed using STLC methodology except that detonized water is substituted for citric acid buffer as the extraction fluid <br /> DISTLC results are not applicable to STLC regulatory lirmts <br /> i)liquid sample that contains greater than—2 vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,z)reporting linut raised due to matnx interference <br /> ' DHS Certification No 1644 Edward Hamilton,Lab Director <br />