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1 <br /> ' CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater CA 95301 Phone (209)384-2930 <br /> Certificate#2480 Fax (209)384-1507 <br /> Advanced Geo Envi ron mental, Inc Client Project ID Rainwater Car Wash Sampled 08-16-02 <br /> of Northern California Reference Number 4987 Received 08-20-02 <br /> 837 Shaw Road Sample Description water Extracted 08-23-02 <br /> ' Stockton, CA 95215 Sample Prep/Analysis Method EPA 5030/8260 Analyzed 08-23-02 <br /> Attn Tim Cuellar Lab Number 4987-1W Reported 08-28-02 <br /> Client Sample ID MW 1 08-16-02 <br /> VOLATILE ORGANICS -EPA METHOD 8260 GCIMS <br /> REPORTING SAMPLE REPORTING SAMPLE <br /> ANALYTE LIMIT' RESULT ANALYTE LIMIT" RESULT <br /> ' /L /L) /L !L <br /> Benzene 050 ND 1,3-Dichloro ro ane 0 50 ND <br /> Bromobenzene 050 ND 2,2-Dichloro ro ane 0 50 ND <br /> Bromochloromethane 060 ND 1,1-Dichloro ro ene 0 50 ND <br /> ' Bromodichloromethane 050 NO cis-1,3-Dlchloro ro ene 050 ND <br /> Bromoform 050 ND trans-1 3-Dichloro re ene 0 50 ND <br /> Bromomethane 050 ND Eth (benzene 050 ND <br /> n-But (benzene 050 NO Hexachlorobutadiene 050 ND <br /> ' sec-But (benzene 050 ND Isopropylbenzene 050 ND <br /> tert-But (benzene 060 ND -Isoprop (toluene 050 ND <br /> Carbon tetrachloride 050 NO Methylene chlonde 050 ND <br /> Chlorobenzene 050 ND Methyl tert-Bu I Ether MTBE 050 420 <br /> Chlorodibromomethane 050 ND Na thalene 050 ND <br /> Chloroethane 050 ND n-Prop (benzene 050 ND <br /> Chloroform 0 50 ND Styrene 050 ND <br /> '. Chloromethane 050 ND 1,1 1,2-Tetrachloroethane 050 ND <br /> 2-Chiorotoluene 050 ND 1 1 2,2,-Tetrachiorethane 0 50 ND <br /> 4-Chlorotoluene 050 ND Tetrachloroethene 0 50 ND <br /> 1,2-Dibromo-3-chloropro ane 050 ND Toluene 0 50 ND <br /> 1 2-Dibromoethane EDB 050 ND 1 2,3-Trichlorobenzene 0 50 ND <br /> Dibromomethane 050 ND 1 2 4-Tnchiorobenzene 0 50 ND <br /> 1,2-Dichlorobenzene 050 ND 1,1,1-Trichloroethane 0 50 ND <br /> 1,3-Dichlorobenzene 050 NO 1,1,2-Trichloroethane 0 50 ND <br /> 1,4-13ichlorobenzene 1150 ND Trichloroethene 150 ND <br /> Dichlorodifluoromethane 050 ND Trichlorofluoromethane 050 ND <br /> 1 1-Dichloroethane 050 NO 1,2 3-Trcchloro ro ane 050 ND <br /> 1 2-Dichloreethane 050 ND 1,2 4-Trtmeth (benzene 0 50 ND <br /> ' 1,1-Dichlorcethene 050 NO 1 3,5-Trimeth (benzene 050 ND <br /> cis-1 2-Dichloroethene 050 ND Vinyl Chloride 050 NO <br /> trans-1 2-Dichloroethene 050 ND Xylenes total 0 50 NO <br /> 1 2-Dichloro ro ane 050 ND <br /> 1 'Report Limit Multiplication Factor 5— <br /> 'Report Limit Multiplication Factor for MTBE 100 <br /> ' "Report limit raised due to matrix interference <br /> Surrogate Recoveries <br /> ' Dibromofluoromethane 143% Toluene-d8 947% <br /> 1 2-Dichioroethane-d4 814% p-Bromofluorobenzene 963% <br /> instrument If] HP 5972 MS <br /> ' Analytes reported as ND were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit=Reporting Limit x Report Limit Multiplication Factor <br /> (Ng/L)= microgram er liter or rts er dlion(ppb) f <br /> 4 i <br /> ' y CYST APPROVED BY 7/�4 <br /> `r Clan J Cone me Ph1111ps I <br /> aboratory Director <br /> 1 E <br /> i <br />