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California Environmental Protection Agency HML # : 960778 to Department of Toxic Substances Control 960800 Hazardous Materials Laboratory (Inorganic Section) 2151 Berkeley Way, Berkeley, CA 94704 Phone: (510) 540-3003 or (ATSS) 571-3003 Collector's Name: NANCY LANCASTER Auth. No. : HMM3119 Site of Sampling: ADVANCED METAL PLATING Activity : SEB 4421 GIANNECHINI Date Collected: 1/24/97 STOCKTON Date Received: 1/27/97 Analytical Samples are digested with 1: 1 HNO3 (and 30% H202 , and 1: 1 HC1 , Procedure: if applicable) over a hot plate. Digests are cooled, filtered EPA-SW 846 and made to final volume with deionized H2O. Metal analysis of the digests is by ICPAES (EPA #6010) . Units are mg/kg. Method: 3050 for solids; 3010 for liquids; 3005 for clean water. HML Number: 960783 960784 960785 960787 960788 Collector's Sample No. : NKL006 NKL007 NKL008 NKLO10 NKLO11 Sample Type: SOLID LIQUID LIQUID LIQUID LIQUID As-Arsenic 12 . 8 <0 . 40 218 <0 . 80 <0 . 40 Ba-Barium 1 . 41 <0. 02 5. 59 3 . 18 0. 16 Be-Beryllium 0 . 19 <0. 01 0. 04 <0. 02 <0 . 01 Cd-Cadmium 1. 51 <0. 04 <0 . 08 <0 . 08 <0 . 04 Co-Cobalt <1. 00 <0 . 20 4 . 72 <0. 40 <0 . 20 Cr-Chromium 39 . 7 <0. 30 >23700 224 48 . 2 Cu-Copper 39 . 3 10. 6 >12900 44 . 7 30. 0 Mo-Molybdenum <1. 50 <0. 30 7 . 57 <0 . 60 <0 . 30 Ni-Nickel 8 . 52 <0. 30 >3020 9 . 52 2 . 60 Pb-Lead 2 . 86 <0. 50 2 . 01 49 . 3 <0 . 50 Se-Selenium 8 . 40 <0 . 80 1.72 <1 . 60 <0. 80 T1-Thallium <7 . 50 <1. 50 60. 7 <3 . 00 <1 . 50 V-Vanadium 1.70 <0. 25 <0. 50 <0. 50 <0 . 25 Zn-Zinc >18600 <0. 15 348 12 . 3 52 . 0 Notes: < = below detection limit of method. > = beyond standard calibration curve; (to be confirmed; an additional report will follow) ICP Analyst Date emist's Signe Date Gurail is .2 Mila s nder Supervisor Date