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April 6, 2007 Lab ID STK732332 <br /> : <br /> Neil Anderson & Associates Customer 3009574 <br /> Quality Control: <br /> Inorganic - Wet Chemistry QC <br /> 4500-H B 03/09/2007:A - PH2O3 Continued... <br /> 03/09/2007:A - PH2O3 All analysis quality controls are within established criteria. <br /> 4500NH3H 03/12/2007:A203 All preparation quality controls are within established criteria, except: <br /> The following note applies to Anunonia-N: <br /> 408 Matrix Spike(MS) or Post Digestion Spike(PDS) has no Acceptance Mange <br /> (DQO) because of high analyte concentration in the sample. Data was accepted based <br /> on the LCS or CCV recovery. <br /> 03/13/2007:B - FI203 All analysis quality controls are within established criteria. <br /> 450ONO3F 03/16/2007:C220 All preparation quality controls are within established criteria. <br /> 04/03/2007:B220 All preparation quality controls are within established criteria, except: <br /> The following note applies to Nitrate + Nitrite as N: <br /> 408 Matrix Spikc(MS) or Post Digestion Spike(PDS) has no Acceptance Range <br /> (DQO) because of high analyte concentration in the sample. Data was accepted based <br /> on the LCS or CCV recovery. <br /> 03/16/2007.0 - FI203 All analysis quality controls are within established criteria. <br /> 04/04/2007:C - FI203 All analysis quality controls are within established criteria. <br /> 5210B 03/09/2007:B204 All preparation quality controls are within established criteria. <br /> 03/14/2007:B - 02201 All analysis quality controls are within established criteria. <br /> 5220B 03/16/2007:A206 All preparation quality controls are within established criteria. <br /> 03/16/2007:A - UV205 All analysis quality controls are within established criteria. <br /> Certification: I certify that this data package is in compliance with NELAC Standards, both <br /> technically and for completeness, except for any conditions listed above. Release of the data <br /> contained in this data package is authorized by the Laboratory Director or his designee, as <br /> verified by the following signature. <br /> FGL ENVIRONMENTAL <br /> KAD:dmb el Dunnahoo, B.S. <br /> Laboratory Director <br /> STK732332: Case Narrative Page 2 <br />