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� •, �o �a pike <br /> ENVIRONMENTAL <br /> Analytical Chemists <br /> March 1, 2011 Lab ID. : STK1131330 <br /> Musca Family Olive Environmental Customer : 341544 <br /> Quality Control-Inorganic <br /> } onstituent Method Date/1D Type Units Conc. QC Data DQO Note <br /> etais <br /> odium 200.7 MS mg/L 12.50 90.6'% 75-125 <br /> (SP 1101818-002) MSD mg/L 12.50 90.0-% 75-125 <br /> MSRPD I mg1L 4,000 0.1% X20.0 <br /> 200.7 02/23/2011102787 CCV ppm 25.00 102% 90-110 <br /> CCB ppm 0.01 1.0 <br /> CCV ppm 25.00 100% 90-110 <br /> CCB Pont 0.05 1.0 <br /> Wet Chem <br /> Solids,Total Dissolved 2540 G 02/18/2011:201886 Blank mg/L ND <20 <br /> LCS mg/L 995.0 l01 % 90-110 <br /> VI 1140355-001)_ Dup I Ma 1 5.7% 10.0 <br /> Solids,Suspended 2540D 0211712011:310248 Blank mg/L ND <1 <br /> LCS mg/L 500.0 95.6% 38-138 <br /> LCS mg/L 500.0 96.6% 38-138 I <br /> STK1131483-002) Du m 1.3% 28.7 <br /> Nitrogen,Total Kjeldahl 351.2 0212112011:201931 Blank mg/L ND <1 <br /> LCS mg/L 12.00 68.5% 41-148 <br /> LCS tng/L 12.00 60.3% 41-148 <br /> MS mg/L 12.00 68.5% 25-149 <br /> (SP 1 101602-001) MSD mg/L 12.00 68.4% 25-149 <br /> MSRPD mWL 12.00 0.09% X25.7 <br /> Nitrate+Nitrite as N 450ONO3F MS mg/L 4.000 97.2% 5-285 <br /> (SP 1101613-001) MSD mglL 4.000 95.6% 5-285 <br /> MSRPD m 4.000 1.7% :30.4 <br /> 450ONO3F 02/21/2011202632 ICB mg/L -0.038 0.1 <br /> ICV mg/L 4.000 106% 90-110 <br /> CCB mg/L -0.039 0.1 ; <br /> CCV mg/L 4.000 106% 90-110 <br /> CCB mg/L -0.034 0.1 <br /> CCV m 4.000 106% 90-110 { <br /> OD 5210B 02/16/2011:300134 RgBlk mg/L -0.15 2 I <br /> RgBlk mg/L -0.17 2 <br /> LCS mg/L 198.0 95,7% 84.6-115 <br /> (STK 113143 7-001) Dup mg/L 2.7% 15.9 <br /> STK113143 7-001 Dup m 7.3% 15.9 <br /> 52108 02/21/2011:300144 CCV mWL 1.000 98,0% 80-120 g <br /> Nitrogen,Total Kjeldahl EPA351.2 02/24/2011:202838 CCB mg/L 0.000 0.2 <br /> CCV mg/L 2.000 95.0% 90-110 <br /> CCB mg/L 0.000 0.2 <br /> CCV mg/L 2.000 l01 °/a 90-I to <br /> Y CCB mg/L 0,000 0.2 <br /> CCV mg/L 2.000 102% 90-110 <br /> CCH mg/L 0.000 0.2 <br /> CCV MWL 2.000 1020/. 90-110 <br /> Definition <br /> lCV :Initial Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> ICB :Initial Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. .'- <br /> MS :Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries <br /> are an indication of how that sam le matrix affects anal a recovery. <br /> Page 9 of 11 I <br /> Corporate Offices B Laboratory Office&Laboratory Office&Laboratory Field Office <br /> 853 Corporation Street 2500 Stagecoach Road 563 E.Undo Avenue Visalia,Callfornla <br /> Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 TEL:5591734-9473 <br /> TEL:8051392-2000 TEL:2091942-0162 TEL:5301343.5818 WNW 55gf737-2399 <br /> FAX'.8051525-4172 FAX:209/942-0423 FAX:530/343-3807 FAX;5591734-8435 <br /> CA NELAP Certification No.a1110CA CA ELAP Cartification No.1563 CA FLAP Cert!£cation No.2670 <br />