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`�O 1N AGCO4pi ENVIRONMENTAL Jk .v 4 Analytical Chemists January 11, 2011 Lab ID : STK1051068 Musco Family Olive Environmental Customer : 3-11544 Quality Control-Inorganic onstituent Method Date11D Type Units Conc. QC Data DQO Note etals odium 200.7 12/3112010:200018 CCV ppm 25.00 95.0% 90-110 CCB ppm -0.15 1.0 CCV ppm 25.00 97,2% 90-110 CCB I pp- -0.09 1.0 200.7 MS mg/L 12.50 102% 75-125 1 (SP 1013217-001) MSD mg/L 12.50 102% 75-125 MSRPD m 798,8 0.01% <20.0 Wet Chem Solids,Total Dissolved 2540 G 12/22/2010:213245 Blank mg1L ND <20 LCS mg/L 995.0 99.9% 90-110 SP 1013046-008 Dup MWL 3.5% 10.0 Solids,Suspended 2540D 12/20/2010:312041 Blank mg/L ND <1 LCS mg/L 500:0 99,0% 38-138 LCS mg/L 500.0 99.5% 38-138 STK1051009-003 Dup m 2.5% 28.7 t Nitrogen,Total Kjeldahl 351.2 12/27/2010:213324 Blank mg/L ND <1 LCS mg/L 12.00 76.9% 41-148 LCS mg/L 12.00 81.3% 41-148 MS mg1L 12.00 81.2% 25-149 (SP 1012942-004) MSD mg/L 12.00 77.5% 25-149 MSRPD m 12.00 4.7% _Q5.7 itrate+Nitrite as N 450ONO3F MS mg/L 4,000 99.7% 5-285 (SP 1013128-001) MSD mg/L 4.000 99.7% 5-285 MSRPD m 4,000 0.04% 630.4 i 450ONO3F 12/30!2010:216858 CCH mg/L -0.022 0.1 CCV mg/L 4.000 102% 90-110 t CCB mg(L -0.028 0.1 CCV mg/L 4,000 102% 90-110 CCB mglL -0.039 0.1 CCV m 4.000 101% 90-110 OD 52106 12/17/2010:300013 RgBlk mg/L 0.60 2 b RgBlk mg/L 0.58 2 b LCS mg/L 198.0 104% 84.6-115 LCS mg/L 198.0 103,% 84.6-115 (STK1051068-001) Dup mg/L 3.1% 15.9 STK1051068-001 Dup m 2.6% 15.9 1EPA351.2 12!2212010:300013 CCV mg/L 1.000 98.0% 80-120 } ,- CCV m 1.000 98.0% 80-120 Nitrogen,Total Kjeldahl 12/30/2010:216813 CCB mg/L 0.000 0.2 r CCV mgLL 2,000 92.0% 90-110 l CCB mg/L 0.000 0.2 CCV m 2.000 108% 90-110 Definition ( CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. I CCB :Continuing Calibration Blank-Analyzed to verify the instrrunent baseline is within criteria, t Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery, MS Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample matrix affects analyte recovery. MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries are an indication of how that sample matrix affects analyte recovery, :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an Dup indication of precision for the preparation and analysis. MSRPD :MS/MSD Relative Percent Difference(RPD)-The MS relative percent difference is an indication ofprecision for the preparation and analysis. Page 9 of I I Corporate Offices&Laboratory Office&Laboratory Office&Laboratory Field Office 853 Corporation Street 2500 Stagecoach Road 563 E.Lindo Avenue Visalia,California Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 TEL:5591734-9473 TEL:8051392-2000 TEL:209/942-0182 TEL:53013435818 Mobile:559f737-2399 FAX:8051525-4172 FAX:2091942-0423 FAX:5301343-3807 FAX:559/734-8435 CA NELAP Certification No.0111 OCA CA ELAP Certification No.1563 CA ELAP Certification No.2670 hi