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a� <br /> ENVIRONMENTAL .A <br /> Analytical Chemists <br /> January 20, 2015 Lab ID : STK1453087 <br /> Musco Family Olive Environmental Customer : 3-11544 <br /> Quality Control-Inorganic <br /> Constituent Method Date/ID Type Units Cone. QC Data DQO Note <br /> Metals <br /> Sodium 200.7 MS mg/L 12.00 81.7% 75-125 <br /> (SP 1500285-002) MSD mg/L 12.00 92.6% 75-125 <br /> MSRPD mg/L 4000 2.1% :�20.0 <br /> 200.7 01/09/15:200440AC CCV ppm 25.00 97.4% 90-110 <br /> CCB ppm -0.05 1 <br /> CCV ppm 25.00 95.0% 90-110 <br /> CCB Min -0.07 1 <br /> Wet Chem <br /> Solids,Total Dissolved 2540CE 01/05/15:20008ICTL Blank mg/L ND <20 <br /> LES mg/L 100, 95.3% 90-110 <br /> STK1453089-001 Dup mg/L 0.3% 5 <br /> Solids,Suspended 2540D 12/31/14:312705CTH Blank mg/L ND <1 <br /> LES mg/L 500.0 97.6% 38-138 <br /> LES mg/L 500.0 96.7% 38-138 <br /> STK1453034-001 Dup mg/L 1.8% 28.7 <br /> Nitrogen,Total Kjeldahl 351.2 01/06/15:200108CJJ Blank mg/L ND <1 <br /> LES mg/L 12.00 86.0% 73-124 <br /> MS mg/L 12.00 54.6% 54-136 <br /> (STK1453038-001) MSD mg/L 12.00 -5.0% 54-136 435 <br /> MSRPD mg/L 12.00 7.2 _<1 435 <br /> itrate+Nitrite as N 450ONO3F MS mg/L 11.27 101% 5-285 <br /> (CH 1479235-001) MSD mg/L 11.27 99.2% 5-285 <br /> MSRPD mg/L 11.27 1.7% <_30.4 <br /> 450ONO3F 01/06/15:200186CJJ CCB mg/L 0.070 0.1 <br /> CCV mg/L 11.27 95.5% 90-110 <br /> CCB mg/L 0.027 0.1 <br /> CCV mg/L 11.27 109% 90-110 <br /> 450ONO3F 01/06/15:200208CJJ ICB mg/L 0.081 0.1 <br /> ICV mg/L 11.27 93.9% 90-110 <br /> CCB mg/L 0.10 0.1 <br /> CCV m 11.27 94.2% 90-110 <br /> BOD 5210B 01/05/15:300006CT CCV mg/L 1.000 98.0% 80720 <br /> CCV m 1.000 97.0% 80-120 <br /> 5210B 12/31/14:300007YKG RgBIk mg/L 0.14 2 <br /> LES mg/L 198.0 93.3% 84.6-115 <br /> (STK1453051-001) Dup mg/L 17.5% 15.9 440 <br /> (STK1453051-001 Du m 31.9% 15.9 440 <br /> itrogen,Total Kjeldahl EPA351.2 01/08/15:200194AMB CCB mg/L 0.087 0.5 <br /> CCV mg/L 5.000 91.5% 90-110 <br /> CCB mg/L 0.015 0.5 <br /> CCV mg/L 5.000 90.9% 90-110 <br /> Definition <br /> ICV :Initial Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> ICB :Initial Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBIk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> MS Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries <br /> are an indication of how that sample matrix affects analyte recovery. <br /> Dup :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an <br /> indication of recision for the preparation and analysis. <br /> Page 9 of 11 <br /> Corporate Offices&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory <br /> 853 Corporation Street 9415 W Goshen i p 2500 Stagecoach Road 563 E.Undo Avenue 3442 Empresa Drive,Suite D W.G h n Avenue <br /> Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 Visalia,CA 93291 <br /> TEL:(805)392-2000 TEL:(209)942-0182 TEL:(530)343-5818 TEL:(805)783-2940 TEL:(559)734-9473 <br /> Env FAX:(805)525-4172/Ag FAX:(805)392-2063 FAX:(209)942-0423 FAX:(530)343-3807 FAX:(805)783-2912 FAX:(559)734-8435 <br /> CA ELAP Certification No.1573 CA ELAP Certification No.1563 CA ELAP Certification No.2670 CA ELAP Certification No.2775 CA ELAP Certification No.2810 <br />