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ENVIRONMENTAL Ali <br /> . , <br /> Analytical Chen-iists <br /> April 9, 2013 Lab ID : STK1332465 <br /> Musco Family Olive Environmental Customer : 3-11544 <br /> Quality Control -Inorganic <br /> onstituent Method Date/ID Type Units Conc. QC Data DQO Note <br /> etals <br /> odium 200.7 MS mg/L 12.00 104% 75-125 <br /> (SP 1303228-001) MSD mg/L 12.00 126% <%s <br /> MSRPD mg/L 798.8 3.8% <20.0 <br /> 200.7 04/01/13:204573AC CCV ppm 25.00 96.9% 90-110 <br /> CCB ppm -0.05 1.0 <br /> CCV ppm 25.00 99.3% 90-110 <br /> CCB ppm -0.04 1.0 <br /> Wet Chem <br /> Solids,Total Dissolved 2540CE 03/26/13:203252CHL Blank mg/L ND <20 <br /> LCS mg/L 995.0 98.2% 90-110 <br /> SP 1302980-001) m L 0.7% 10.0 <br /> Solids,Suspended 2540D 03/22/13:310460KJB Blank mg/kg ND <1 <br /> LCS mg/kg 500.0 98.0% 38-138 <br /> LCS mg/kg 500.0 99.1% 38-138 <br /> STK1332469-001 Dup m 0.8% 28.7 <br /> Nitrate 300.0 03/22/13:203296CHL LCS mg/L 20.00 93.9% 90-110 <br /> MS mg/L 400.0 105% 93-113 <br /> (CC 1380884-001) MSD mg/L 400.0 101 % 93-113 <br /> MSRPD mg/L 100.0 4.0% _<4 <br /> 300.0 03/22/13:204390CHL CCB ppm 0.039 0.4 <br /> CCV ppm 20.00 97.4% 90-110 <br /> CCB ppm 0.040 0.4 <br /> CCV ppm 20.00 98.7% 90-110 <br /> CCB ppm 0.036 0.4 <br /> CCV PPm 20.00 97.1 % 90-110 <br /> Nitrogen,Total Kjeldahl 351.2 04/05/13:203707CJJ Blank mg/L ND <1 <br /> LCS mg/L 12.00 73.7% 73-124 <br /> MS mg/L 12.00 63.0% 54-136 <br /> (SP 1302932-001) MSD mg/L 12.00 60.2% 54-136 <br /> MSRPD mg/L 12.00 4.6% <27 <br /> OD 5210B 03/22/13:300252CTH RgBlk mg/L 0.11 2 <br /> RgBlk mg/L 0.15 2 <br /> LCS mg/L 198.0 105% 84.6-115 <br /> LCS mg/L 198.0 108% 84.6-115 <br /> (STK 1332484-001) Dup mg/L 2.1% 15.9 <br /> (STK1332484-001) Dup mg/L 1.6% 15.9 <br /> (STK1332484-001 Dup mg/L 12.8% 15.9 <br /> 5210B 03/27/13:300257JK CCV m 1.000 101% 80-120 <br /> Nitrogen,Total Kjeldahl EPA351.2 04/08/13:204927AMB CCB mg/L 0.210 0.5 <br /> CCV mg/L 1.000 95.2% 90-110 <br /> CCB mg/L 0.131 0.5 <br /> CCV mg/L 1.000 95.5% 90-110 <br /> Definition <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> MS Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries <br /> are an indication of how that sample matrix affects analyte recovery. <br /> Dup :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an <br /> indication of precision for the preparation and analysis. <br /> MSRPD :M S/MSD Relative Percent Difference(RPD)-The MS relative percent difference is an indication of precision for the preparation <br /> and anal sis. <br /> nelac Page 9 of 11 <br /> Corporate Offices&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory Field Office <br /> 853 Corporation Street 2500 Stagecoach Road 563 E.Lindo Avenue 3442 Empresa Drive,Suite D Visalia,California <br /> Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 TEL:(559)734-9473 <br /> TEL:(805)392-2000 TEL:(209)942-0182 TEL:(530)343-5818 TEL:(805)783-2940 Mobile:(559)737-2399 <br /> Env FAX:(805)525-4172/Ag FAX:(805)392-2063 FAX:(209)942-0423 FAX:(530)343-3807 FAX:(805)525-4172 FAX:(559)734-8435 <br /> CA NELAP Certification No.01110CA CA ELAP Certification No. 1563 CA ELAP Certification No.2670 CA ELAP Certification No.2775 <br />