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ENVIRONMENTACW AGRICULTURAL <br /> Analytical ChemisLs <br /> October 4, 2018 Lab ID : STK1853988 <br /> Musco Family Olive Environmental Customer : 3-11544 <br /> Quality Control -Inorganic <br /> Constituent Method Date/ID 1'3pc Units Conc. QC Data DQO Note <br /> Metals <br /> Sodium 200.7 MS mg/L 12.00 99.1% 75-125 <br /> (SP 1813042-002) MSD mg/L 12.00 96.2% 75-125 <br /> MSRPD m 800.0 0.7% 1520.0 <br /> 200.7 10/02/18:214440AC CCV ppm 25.00 101% 90-110 <br /> CCB ppm 0.11 1 <br /> CCV ppm 25.00 103% 90-110 <br /> CCB ppm 0.11 1 <br /> CCV ppm 25.00 106% 90-110 <br /> CCB ppru 0.10 1 <br /> Wet Chem <br /> Total Dissolved Solids(TFR) 2540CE 09/28/18:211648CTL Blank mg/L ND <20 <br /> LCS mg/L 993.1 99.8% 90-110 <br /> (CC 1883013-001) Dup mg/L 0.9% 5 <br /> (CC 1883013-003) Dup I m 1.5% 5 <br /> Solids,Suspended 1-5401) 09/26/18:312233CTH Blank mg/L ND <1 <br /> LCS mg/L 500.0 98.9% 61-112 <br /> LCS mg/L 500.0 99.6% 61-112 <br /> (STK1853925-001) Dup mg/L 0.7% 20 <br /> (STK1853985-001) Du m 40.7% 20 440 <br /> Nitrogen,Total Kjeldahl 3512 10/02/18:211727jmg Blank mg/L ND <0.5 <br /> LCS mg/L 12.00 - 77.0% 73-124 <br /> MS mg/L 12.00 71.9% 54-136 <br /> (VI 1845234-001) MSD mg/L 12.00 51.4% 54-136 435 <br /> MSRPD m 12.00 31.9% 527 435 <br /> itrate+Nitrite as N 450ONO3F MS mg/L 28.17 36.7% 5-285 <br /> (CH 1878593-001) MSD mg/L 28.17 37.3% 5-285 <br /> MSRPD m 28.17 1.4% :530.4 <br /> 450ONO3F 09/27/18:214250JDD CCB mg/L 0.158 0.2 <br /> CCV mg/L 11.27 96.3% 90-110 <br /> CCB mg/L 0.151 0.2 <br /> CCV m 11.27 96.6% 90-110 <br /> OD 10B 09/26/18:300368sm RgBlk mg/L 0.06 2 <br /> LCS mg/L 198.0 101% 84.6-115 <br /> (STK1853912-001) Dup mg/L 0.6% 15.9 <br /> (S FK1853912-001) Dup mg/L 23.0% 15.9 440 <br /> (STK1853912-001) mg/L 68.6% 15.9 440 <br /> 5210B 10/01/18:300372ct CCV mg/L 1.000 99.0% 80-120 <br /> CCV m 1.000 100% 80-120 <br /> Nitrogen,Total Kjeldahl EPA351.2 10/02/18:214468JDD CCB mg/L 0.232 0.5 <br /> CCV mg/L 5.000 97.6% 90-110 <br /> CCB mg/L 0.057 0.5 <br /> CCV mg/L 5.000 90.2% 90-110 <br /> Definition <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> MS Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries <br /> are an indication of how that sample matrix affects analyte recovery. <br /> Dup :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an <br /> indication of precision for the preparation and analysis. <br /> MSRPD :MS/MSD Relative Percent Difference(RPD)-The MS relative percent difference is an indication of precision for the preparation <br /> and analysis. <br /> Page 9 of 11 <br /> Corporate Offices&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory <br /> 853 Corporation Street 2500 Stagecoach Road 563 E.Lindo Avenue 3442 Empresa Drive,Suite D 9415 W.Goshen Avenue <br /> Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 Visalia,CA 93291 <br /> TEL:(805)392-2000 TEL:(209)942-0182 TEL:(530)343-5818 TEL:(805)783-2940 TEL:(559)734-9473 <br /> Env FAX:(805)525-4172/Ag FAX:(805)392-2063 FAX:(209)942-0423 FAX:(530)343-3807 FAX:(805)783-2912 FAX:(559)734-8435 <br /> CA ELAP Certification No.1573 CA ELAP Certification No.1563 CA ELAP Certification No.2670 CA ELAP Certification No.2775 CA ELAP Certification No.2810 <br />