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Analytical Chemists <br /> January 2, 2018 Lab ID : STK1755318 <br /> Musco Family Olive Environmental Customer : 3-11544 <br /> Quality Control-Inorganic <br /> Constituent Method Date/ID Type Units Cone. QC Data DQO Note <br /> Metals <br /> Sodium 200.7 MS mg/L 12.00 95.5% 75-125 <br /> (STK1755336-003) MSD mg/L 12.00 93.2% 75-125 <br /> MSRPD m 4000 0.5% _<20.0 <br /> 200.7 12/09/17:218503AC CCV ppm 25.00 97.1% 90-110 <br /> CCB ppm -0.11 1 <br /> CCV ppm 25.00 96.5% 90-110 <br /> CCB plan 0.05 1 <br /> Wet Chem <br /> Total Dissolved Solids(TFR) 2540CE 12/13/17:214857CTL Blank mg/L ND <20 <br /> LCS mg/L 992.3 100% 90-110 <br /> (STK1755317-001) Dup mg/L. 0.4% 5 <br /> STK1755297-001 Dup m 2.1% 5 <br /> Solids,Suspended 2540D 12/07/17:312604AUS Blank ni ND <1 <br /> LCS mg/L. 500.0 96.6% 61-112 <br /> LCS mg/L 500.0 95.7% 61-112 <br /> (STY,]755348-001) Dup mg/L 4.1% 20 <br /> (STK1755367-001) Dup I m 12.8% 20 <br /> Nitrogen,Total Kjeldahl 351.2 12/I1/17:214718jmg Blank mg/L ND <0.5 <br /> LCS mg/L 12.00 84.2% 73-124 <br /> MS mg/L 12.00 85,2% 54-136 <br /> (STK1755227-001) MSD mg/L 12.00 83.5°/ 54-136 <br /> MSRPD ni 12.00 1.9% <_27 <br /> Nitrate+Nitrite as 450ONO3F MS mg/L 28.04 37.6% 5-285 <br /> (Vi 1746234-001) MSD mg/L 28.04 38.3% 5-285 <br /> MSRPD m 28.04 1.9% <30.4 <br /> 450ONO3F 12/08/17:218459JDD CCB mg/L 0.067 0.1 <br /> CCV mg/L 11.22 97.0% 90-110 <br /> CCB mg/L 0.091 0.1 <br /> CCV m 11.22 98.0% 90-110 <br /> OD 5210B 12/07/17:300413SM RgBlk mg/L 1.0 2 735 <br /> LCS mg/L 198.0 106% 84.6-115 <br /> (STK1755347-001) Dup mg/L 13.4% 15.9 <br /> (STK1755347-001) Dup mg/L 5.6% 15.9 <br /> STK1755347-00I Dun m Z0% 15.9 <br /> 5210B 12/12117:300415CT CCV mg/L 1.000 100% 80-120 <br /> CCV m 1,000 99.0% 80-120 <br /> Nitrogen,Total Kjeldahl F,PA351.2 12/13/17:218627AMB CCH mgt -0.464 0.5 <br /> CCV mg/L 5.000 95.2% 90-110 <br /> CCB mg/L 0.247 0.5 <br /> CCV m 5.000 98.0% 90-110 <br /> Definition <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> MS :Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries <br /> are an indication of how that sample matrix affects analyte recovery. <br /> Du :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an <br /> Dup indication of precision for the preparation and analysis. <br /> MSRPD .MS/MSD Relative Percent Difference(RPD)-The MS relative percent difference is an indication of precision for the preparation <br /> and analysis. <br /> ND :Non-detect-Result was below the D O listed for the analyte. <br /> Page 9 of 11 <br /> Corporate Offices&Laboratory Office is Laboratory Off...&Laboratory Office&Laboratory Office&Laboratory <br /> 853 Corporation Street 2500 Stagecoach Road 563 E.Linde Avenue 3442 Empresa Drive,Suite D 9415 W.Goshen Avenue <br /> Some Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 Visalia,CA 93291 <br /> TEL:(805)392-2000 TEL:(209)942-0182 TEL:(530)343-5818 TEL:(805)783-2940 TEL:(559)734-9473 <br /> Env FAX:(805)525-4172/Ag FAX:(805)392-2063 FAX(209)942-0423 FAX:(530)3433807 FAX:(805)783-2912 FAX:(559)734-8435 <br /> CA ELAP Certification No.1573 CA ELAP Certification No.1563 CA ELAP Certification No.2670 CA ELAP Certification No.2775 CA ELAP Certification No.2810 <br />