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ENVIRO . , <br /> Analytical Chemists <br /> December 12, 2018 Lab ID : STK1856681 <br /> Musco Family Olive Environmental Customer : 3-11544 <br /> Quality Control-Inorganic <br /> Constituent Method Date/1D Type Units Conc. QC Data DQO Note <br /> Metals <br /> Sodium 200.7 Ms mg/L 12.00 23.6% <'/a <br /> (CH 1879877-004) MSD mg/L 12.00 -1.8% <'/4 <br /> MSRPD m 4000 2.2% 520.0 <br /> 200.7 11/27/18:217305AC CCV ppm 25.00 104% 90-110 <br /> CCB ppm 0.04 1 <br /> CCV ppm 25.00 103% 90-110 <br /> CCB ppm 0.1 1 <br /> CCV ppm 25.00 103% 90-110 <br /> CCB ppm 0.07 1 <br /> Wet Chem <br /> Total Dissolved Solids(TFR) 2540CE 11/26/18:213916CTL Blank mg/L ND <20 <br /> LCS mg/L 993.1 100% 90-110 <br /> (SP 1815367-004) Dup mg/L 0.07% 5 <br /> (SP 1815367-005) Dup mg/L 0.6% 5 <br /> Blank mg/L ND <20 <br /> LCS mg/L 993.1 97.0% 90-110 <br /> (CH 1879877-005) Dup mg/L 0.9% 5 <br /> CH 1879877-006 Dup m 0.6% 5 <br /> Solids,Suspended 2540D 11/21/18:312663AUS Blank mg/L ND <1 <br /> LCS mg/L 500.0 96.2% 61-112 <br /> LCS mg/L 500.0 94.8% 61-112 <br /> (STK1856790-001) Dup mg/L 4.0% 20 <br /> STK1856718-001) Dup m 7.5% 20 <br /> Nitrogen,Total Kjeldahl 351.2 11/26/18:213899jmg Blank mg/L ND <0.5 <br /> LCS mg/L 12.00 84.2% 73-124 <br /> MS mg/L, 12.00 49.5% 54-136 435 <br /> (STK1856585-002) MSD mg/L 12.00 64.0% 54-136 <br /> MSRPD mg/L 12.00 27.0% <27 <br /> Nitrate+Nitrite as N 450ONO3F MS mg/L 28.18 39.6% 5-285 <br /> (VI 1846315-001) MSD mg/L 28.18 40.0% 5-285 <br /> MSRPD m 28.18 0.8% <30.4 <br /> 450ONO3F 11/21/18:217125JDD CCB mg/L 0.008 0.2 <br /> CCV mg/L 11.27 101% 90-110 <br /> CCB mg/L 0.043 0.2 <br /> CCV m 11.27 99.0% 90-110 <br /> OD 5210B 11/20/18:300445af RgBlk mg/L 0.61 2 <br /> LCS mg/L 198.0 100% 84.6-115 <br /> (STK1856671-001) Dup mg/L 12.2% 15.9 <br /> (STK1856671-001) Dup mg/L 9.1% 15.9 <br /> (STK1856671-001) Dup mg/L 20.6% 15.9 440 <br /> (STK1856671-001) Dup m 49.8% 15.9 440 <br /> 5210B 11/25/18:300455af CCV mg/L 1.000 100% 80-120 <br /> CCV m 1.000 98.0% 80-120 <br /> Nitrogen,Total Kjeldahl EPA351.2 11/28/18:217352JDD CCB mg/L 0.293 0.5 <br /> CCV mg/L 5.000 103% 90-110 <br /> CCB mg/L 0.254 0.5 <br /> CCV m 5.000 103% 90-110 <br /> Definition <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> Ms Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> Page 9 of 1 I <br /> Corporate Offices&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory Office&Laboratory <br /> 853 Corporation Street 2500 Stagecoach Road 563 E.Lindo Avenue 3442 Empresa Drive,Suite D 9415 W.Goshen Avenue <br /> Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 Visalia,CA 93291 <br /> TEL:(805)392-2000 TEL:(209)942-0182 TEL:(530)343-5818 TEL:(805)783-2940 TEL:(559)7349473 <br /> Env FAX:(805)525-4172/Ag FAX:(805)392-2063 FAX:(209)942-0423 FAX:(530)343-3807 FAX:(805)783-2912 FAX:(559)734-8435 <br /> CA ELAP Certification No.1573 CA ELAP Certification No.1563 CA ELAP Certification No.2670 CA ELAP Certification No.2775 CA ELAP Certification No.2810 <br />