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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 04/10/20 21:23 <br /> Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AAD0071-EPA 9040B <br /> Duplicate(A^D0071-DUPl) Source:2004007-01 Prepared&Analyzed:04/10/20 <br /> pH 10.352 0.10000 pH Units 10.267 0.824 20 <br /> Duplicate(A^D0071-DUP2) Source:2004042-01 Prepared&Analyzed:04/10/20 <br /> pH 12.576 0.10000 pH Units 12.551 0.199 20 <br /> Duplicate(A^D0071-DUP3) Source:2004043-01 Prepared&Analyzed:04/10/20 <br /> pH 12.560 0.10000 pH Units 12.507 0.423 20 <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 7 of 19 <br />